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Journal of Analytical Atomic Spectrometry
Journal Prestige (SJR): 1.066 ![]() Citation Impact (citeScore): 3 Number of Followers: 8 ![]() ISSN (Print) 0267-9477 - ISSN (Online) 1364-5544 Published by RSC ![]() |
- Precise measurement of 40K isotopic anomalies in small samples using TIMS
with a 1013 Ohm amplifier-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00059A, PaperYingnan Zhang, Siwei Wang, Jia Liu, Bing Yang, Liping Qin
The paradox of volatile depletion in terrestrial planets is critical to the early evolution of planets and the emergence of life. However, the depletion mechanism of volatiles, such as K,...
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- Development of an Optimised Method for Measurement of Iodine-129 in
Decommissioning Wastes Using ICP-MS/MS-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00045A, PaperŽilvinas Zacharauskas, Phillip E Warwick, Ben C. Russell, David Reading, Ian William Croudace
Accurate, low-level measurement of the long-lived fission product 129I is important for waste characterisation and long-term monitoring of waste facilities and the surrounding environment. Inductively coupled plasma mass spectrometry (ICP-MS)...
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- Reduction of Surface Charging Effects in Laser Ablation Ionisation Mass
Spectrometry through Gold Coating-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00078H, Technical NoteOpen Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Salome Gruchola, Andreas Riedo, Peter Keresztes Schmidt, Coenraad P. de Koning, Luca N. Knecht, Marek Tulej, Frances Westall, Peter Wurz
In femtosecond Laser Ablation Ionisation Mass Spectrometry (fs-LIMS) short laser pulses are used to ablate, atomise, and ionise solid sample material shot-by-shot. When ablating non-conductive samples electric charging of the...
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- Rapid nondestructive assessment of degrees of sensitization of 5456
aluminum alloys using laser-induced breakdown spectroscopy (LIBS) with
multivariate analysis-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00017F, PaperLei Liu, Xi Huang, Haoyu Dong, Aofei Mao, Peizi Li, Bai Cui, Jean-François Silvain, Yong-Feng Lu
The 5xxx series aluminum (Al) – magnesium (Mg) alloys are extensively used in marine transportation and naval ships due to their high strength-to-weight ratios and great corrosion resistance properties. However,...
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- Applicability of microwave induced plasma optical emission spectrometry
for wear metal determination in lubricant oil using a multinebulizer-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00093A, Technical NoteSergio J. Abellán-Martín, Miguel Ángel Aguirre, Antonio Canals
In this work, the determination of different metals (i.e., Al, Cr, Cu, Mn, Ni and V) in engine lubricating oils by microwave plasma atomic emission spectrometry (MP AES) has been...
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- Fast determination of electrolyte elements in human blood plasma using
surface-enhanced laser-induced breakdown spectroscopy combined with gel
film method-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00123G, PaperYuanhang Wang, Yang Bu, Biao Yang, Yachao Cai
Electrolyte elements in human blood plasma play an important role in maintaining the osmotic pressure and acid-base balance of body fluids. Rapid and accurate detection of electrolyte concentrations in blood...
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- Machine Learning Analysis to Classify Nanoparticles from Noisy spICP-TOFMS
Data-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00081H, PaperOpen Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Raven L. Buckman, Alexander Gundlach-Graham
Single-particle inductively coupled plasma time-of-flight mass spectrometry (spICP-TOFMS) is a promising method for the quantification and classification of anthropogenic and natural nanoparticle (NP) types based on measured multi-elemental compositions of...
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- Exploration of LIBS as a novel and rapid elemental mapping technique of
nuclear fuels in the form of surrogate TRISO particles-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00034F, PaperBenjamin T Manard, Hunter B. Andrews, C. Derrick Quarles Jr., Veronica C. Bradley, Peter Doyle, N. Alex Zirakparvar, Daniel R. Dunlap, Cole R. Hexel
Laser-induced breakdown spectroscopy (LIBS) was employed to characterize coatings on surrogate fuel particles. Tri-structural isotropic (TRISO) particles are a proposed nuclear fuel alternative for high temperature reactors. These particles are...
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- Classification of uneven steel samples by laser induced breakdown
spectroscopy based on a Bessel beam-
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Abstract:J. Anal. At. Spectrom., 2023, Advance Article
DOI : 10.1039/D3JA00064H, PaperWenhao Yan, Jiaxin Lv, Chenwei Zhu, Qingzhou Li, Ji Chen, Lizhu Kang, Bing Lu, Xiangyou Li
The combination of a Bessel beam and LIBS is an effective method for rapidly detecting uneven samples in industry, which has higher accuracy and stability under fewer spectra.
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- Development and industrial application of LIBS-XRF coal quality analyzer
by combining PCA and PLS regression methods-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00015J, PaperZhihui Tian, Jiaxuan Li, Shuqing Wang, Yu Bai, Yang Zhao, Lei Zhang, Peihua Zhang, zefu ye, zhujun zhu, Wangbao Yin, Suotang Jia
Rapid and stable analysis of coal quality for fine management of coal is essential for the clean and efficient utilization of coal in thermal power plants. In this work, a...
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- Chemical characterization of automobile windshield glass samples by
nuclear and radio-analytical techniques namely SEM-EDX, ED-XRF, PIXE,
PIGE, and INAA and potential of external (in air) PIGE and INAA in
conjunction with chemometrics for glass forensics-
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Abstract:J. Anal. At. Spectrom., 2023, Advance Article
DOI : 10.1039/D3JA00006K, PaperVishal Sharma, Raghunath Acharya, Arnab Sarkar, Hemlata K. Bagla, Pradeep Kumar Pujari
Glass forensics utilizing major elements from external PIGE and trace elements from INAA in conjunction with principal component analysis.
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- Atomic spectrometry update: review of advances in atomic spectrometry and
related techniques-
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Abstract:J. Anal. At. Spectrom., 2023, 38,974-999
DOI : 10.1039/D3JA90013D, Atomic Spectrometry UpdateE. Hywel Evans, Jorge Pisonero, Clare M. M. Smith, Rex N. Taylor
This review covers advances in atomic spectrometric techniques, including atomic emission, absorption, fluorescence and mass spectrometry. Material on speciation and coupled techniques is not covered as this is included in a separate ASU review.
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- Mercury determination in bioresorbable calcium phosphate using a new
electrothermal vaporization system coupled to ICP-MS-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1000-1006
DOI : 10.1039/D2JA00414C, Technical NoteJussiane S. Silva, Graciela M. Heidrich, Bruno O. Poletto, Jose N. G. Paniz, Valderi L. Dressler, Erico M. M. Flores
A new ETV system coupled to ICP-MS was developed to determine Hg at the ultra-trace level in bioresorbable calcium phosphate-based ceramic materials.
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- Determination of broadband-light atomic absorption through interferometric
spectrometry with a spatial heterodyne spectrometer-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1088-1096
DOI : 10.1039/D2JA00367H, PaperXunyu Li, Jens Riedel, Yi You
A spatial heterodyne spectrometer (SHS) was combined with a flame atomic absorption (FAA) setup to reveal the analytical potential of SHS to be used as a tool for high-resolution atomic absorption studies.
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- The efficiency of Hg cold vapor generation and its influence on Hg isotope
analysis by MC-ICP-MS-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1076-1087
DOI : 10.1039/D3JA00056G, PaperMiao Shi, Bridget A. Bergquist, Anwen Zhou, Yaqiu Zhao, Ruoyu Sun, Jiubin Chen, Wang Zheng
Non-quantitative Hg cold-vapor generation can compromise the accuracy of Hg isotope analysis, and it should be monitored and optimized by performing matrix separation, adopting the design of gas–liquid separators, and tuning the sample uptake rate.
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- The feasibility of using a pyrite standard to calibrate the sulfur isotope
ratio of marcasite during SIMS analysis-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1016-1020
DOI : 10.1039/D3JA00009E, PaperRucao Li, Xiao-Lei Wang, Yue Guan, Jing Gu, Lan-Lan Tian
Marcasite (FeS2, orthorhombic) is a dimorph of pyrite (FeS2, isometric), which has been reported in many kinds of ore deposits and sedimentary rocks.
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- Evaluation of the digestion capability of ammonium bifluoride for the
determination of major and trace elements in Ti-rich minerals by ICP-MS-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1146-1154
DOI : 10.1039/D3JA00012E, PaperHong Liu, Zhaochu Hu, Tao He, Wen Zhang, Keqing Zong, Tao Luo, Xiaoyun Qiu, Yang Gao, Mufei Li
An efficient digestion method for the determination of major and trace elements in Ti-rich minerals by ICP-MS.
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- Denoising preprocessing using novel wavelet threshold functions in
laser-induced breakdown spectroscopy based on fiber laser-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1032-1042
DOI : 10.1039/D2JA00345G, PaperBohan Xu, Zhanjian Lin, Zhiying Xu, Xiaotao Yan, Xinying Peng, Chuangkai Li, Yuzhi Qin, Jiaming Li, Nan Zhao, Qingmao Zhang
Fiber lasers have great advantages in long-time operations and stable power, showing great potential in laser-induced breakdown spectroscopy (LIBS) for industrial online diagnosis.
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- A newly synthesized reference material for in situ sulfur isotope
measurement of sphalerite using laser ablation MC-ICP-MS-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1065-1075
DOI : 10.1039/D2JA00394E, PaperXiaojuan Nie, Zhian Bao, Chunlei Zong, Nan Lv, Kaiyun Chen, Honglin Yuan
The PAS-synthesized sphalerite has a homogeneous sulfur isotopic composition and is suitable to be a matrix-matched reference material for in situ S isotope measurements of sphalerite.
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- Precise determination of 204Pb-based isotopic ratios in environmental
samples by quadrupole inductively coupled plasma mass spectrometry-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1057-1064
DOI : 10.1039/D2JA00424K, PaperOpen Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Marco Grotti, Maria Alessia Vecchio, Dalia Gobbato, Matilde Mataloni, Francisco Ardini
Precise and accurate measurement of 204Pb-based isotopic ratios by quadrupole ICP-MS at the part-per-billion concentration level was achieved.
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- In situ Sn isotope analysis of cassiterite (SnO2) by nanosecond laser
ablation MC-ICP-MS-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1043-1056
DOI : 10.1039/D3JA00010A, PaperJia-Xin She, Weiqiang Li, Shichao An, Tao Yang, Rongqing Zhang
This study proposes a new analytical protocol for in situ Sn isotope analysis of cassiterite using a nanosecond laser ablation system and a natural cassiterite reference material.
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- Efficient and robust image registration for two-dimensional micro-X-ray
fluorescence measurements-
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Abstract:J. Anal. At. Spectrom., 2023, 38,1021-1031
DOI : 10.1039/D2JA00347C, PaperOpen Access
  This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.Felix Bock, Andreas Gruber, Kerstin Leopold, Henning Bruhn
Solving image registration problem in micro-X-ray uorescence spectrometry (µ-XRF) is a first step towards application of multi-image super-resolution technique.
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- Experimental determination of ruthenium L-shell fluorescence yields and
Coster–Kronig transition probabilities-
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Abstract:J. Anal. At. Spectrom., 2023, Advance Article
DOI : 10.1039/D3JA00085K, PaperOpen Access
  This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.Nils Wauschkuhn, Katja Frenzel, Burkhard Beckhoff, Philipp Hönicke
Fluorescence yields and Coster–Kronig factors of the ruthenium L-shell are determined experimentally for the first time with reliable uncertainty budgets.
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- Study on a modified spectral standardization method and quantitative
analysis of cement based on microwave plasma torch-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00121K, PaperDengjie Yu, Haoze Wei, Yarui Li, Yibo Shao, Wei Jin, Bingwen Yu
In this study, we used a powder aerosol generator (PAG) to introduce cement powder aerosol directly into a microwave plasma torch (MPT) for quantitative analysis, which demonstrated the feasibility of...
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- Rapid isotopic analysis of uranium, plutonium, and americium in
post-detonation debris simulants by RIMS-
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Abstract:J. Anal. At. Spectrom., 2023, Advance Article
DOI : 10.1039/D3JA00096F, PaperOpen Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Michael R. Savina, Danielle Ziva Shulaker, Brett H. Isselhardt, Gregory A. Brennecka
Uranium interference is a major problem in conventional 238Pu analysis. In RIMS, a slight detuning of the resonance laser extinguishes the Pu signal so that the 238U interference can be accurately quantified and subtracted.
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- Detection of metallothionein as melanoma marker by LA-ICP-MS combined with
sample pretreatment by magnetic particles coated with an imprinted
polymeric layer-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00065F, PaperKristyna Veverkova, Kristyna Pavelicova, Marcela Vlcnovska, Marketa Vejvodova, Vratislav Horák, Viktor Kanicky, Vojtech Adam, Tomas Vaculovic, Marketa Vaculovicova
Effective detection and sensitive quantification of disease markers enable a better understanding of processes leading to disease development. Therefore, we present an approach that combines the excellent selective recognition capabilities...
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- Investigation of matrix effects in nitrogen microwave inductively coupled
atmospheric-pressure plasma mass spectrometry (MICAP-MS) for trace
elemental analysis in steels-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00088E, PaperOpen Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Alexander Winckelmann, Janina Roik, Sebastian Recknagel, Carlos Abad, Zengchao You
We investigated the performance of nitrogen microwave inductively coupled atmospheric-pressure plasma mass spectrometry (MICAP-MS) under matrix effects and its applicability for trace elemental analysis in steels. Influences of different gas...
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- Characterisation of gas cell reactions for 70+ elements using N2O for ICP
tandem mass spectrometry measurements-
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Abstract:J. Anal. At. Spectrom., 2023, Advance Article
DOI : 10.1039/D3JA00025G, PaperOpen Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Shaun T. Lancaster, Thomas Prohaska, Johanna Irrgeher
Gas cell interactions of 73 elements with nitrous oxide (N2O) have been evaluated using inductively coupled plasma tandem mass spectrometry (ICP-MS/MS). Recommendations for the reduction of interferences are provided.
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- Online monitoring of atmospheric Krypton-85 with hourly time resolution
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D2JA00318J, PaperYanQing Chu, Wen-Hao Wang, Xi-Ze Dong, Chao Gao, Ji-Qiang Gu, Shui-Ming Hu, Wei Jiang, Si-Yu Liu, Zheng-Tian Lu, Florian Ritterbusch, Guo-Min Yang, Lei Zhao
85Kr is a major radioactive byproduct released during nuclear fuel reprocessing and an important atmospheric indicator for nuclear safety and environmental monitoring. In this work, we report on online monitoring...
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- An optimization method based on spatial confinement for direct detection
of laser-induced particle flow-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00041A, PaperHongjie Chen, Meirong Dong, Junbin Cai, Zihan Shang, Zhichun Li, Feiqiang Tang, Jidong Lu
Laser-induced breakdown spectroscopy (LIBS) has the advantages of on-line, rapid and multi-element synchronous detection. It can be applied to real-time and rapid properties detection of particle flow. However, the instability...
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- Chemical vapour generation assisted by Cr3+/KCN coupled to atomic
fluorescence spectrometry for ultrasensitive determination of cadmium in
water and rice samples-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00083D, PaperBarbora Stadlerova, Linda Sagapova, Stanislav Musil
A methodology for cadmium determination at ultratrace levels based on chemical vapour generation (CVG) coupled to atomic fluorescence spectrometry (AFS) was developed. Cd volatile species were generated in a four...
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- Determination of trace elements in mineral water by MIP OES using the
Marin-5 nebulization system-
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Abstract:J. Anal. At. Spectrom., 2023, Advance Article
DOI : 10.1039/D3JA00068K, Technical NoteAlexsandro S. Martins, Heronides Adonias Dantas Filho, Kelly G. Fernandes Dantas
In this study, three analytical procedures for the determination of inorganic constituents in mineral water were performed.
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- Parallel-beam wavelength-dispersive X-ray emission spectrometer for high
energy resolution in-air micro-PIXE analysis-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00019B, PaperOpen Access
  This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.Kristina Isaković, Marko Petric, Ava Rajh, Zdravko Rupnik, Mirko Ribič, Klemen Bučar, Primož Pelicon, Paula Pongrac, Valentina Bočaj, Matjaž Kavčič
A new parallel-beam wavelength dispersive (PB-WDS) X-ray emission spectrometer was constructed at the external proton beamline at the Microanalytical Centre of the Jožef Stefan Institute in Ljubljana. The spectrometer combines...
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- Detection of lead in water at ppt levels using resin-enrichment combined
with LIBS-LIF-
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Abstract:J. Anal. At. Spectrom., 2023, Advance Article
DOI : 10.1039/D3JA00057E, PaperXuelin Wen, Zhenlin Hu, Junfei Nie, Zhen Gao, Deng Zhang, Lianbo Guo, Shixiang Ma, Daming Dong
A simple and ultrasensitive method for detecting Pb2+ using resin-enrichment combined with laser-induced breakdown spectroscopy assisted by laser-induced fluorescence.
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- In situ Lu-Hf geochronology with LA-ICP-MS/MS analysis
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D2JA00407K, PaperShi-Tou Wu, Hao Wang, Yue-Heng Yang, Junlong Niu, Zhongwu Lan, Liang-Liang Zhang, Chao Huang, Lie-Wen Xie, Lei Xu, Jin-Hui Yang, Fu-Yuan Wu
Lu–Hf geochronology is useful for constraining the evolution of geological systems. In this study, in situ LA–ICP–MS/MS Lu–Hf dating technique was successfully applied to Paleozoic-Precambrian xenotime, apatite and garnet. For...
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- Laboratory X-ray Emission Spectrometer for Phosphorus Kα and Kβ Study of
Air-Sensitive Samples-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00053B, PaperJared E. Abramson, William M. Holden, Ricardo Rivera-Maldonado, Alexandra Velian, Brandi M. Cossairt, Gerald T. Seidler
The analytical chemistry of phosphorus-containing materials is often impeded by the long measurement times and relatively large sample masses needed for 31P NMR spectroscopy, by the scarcity and access limitations...
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- High-efficiency X-ray emission spectroscopy of cold-compressed Fe2O3 and
laser-heated pressurized FeCO3 using a von Hámos spectrometer-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00014A, PaperOpen Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Christian Albers, Robin Sakrowski, Nicola Thiering, Lélia Libon, Georg Spiekermann, Johannes M. Kaa, Hlynur Gretarsson, Martin Sundermann, Metin Tolan, Max Wilke, Christian Sternemann
X-ray spectroscopy of iron-bearing compounds under high pressure and high temperature is an important tool to understand geological processes in the deep Earth. However, the sample environment using a diamond...
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- Gas Temperature Measurement by Atomic Line Broadening Using LIBS Technique
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D3JA00044C, PaperErcong Gao, Renmin Wei, Dayuan Zhang, Zhifeng Zhu, Qiang Gao, Bo Li
Accurate temperature measurement of the gas flow field is of great significance in theoretical research and engineering applications. Here, we found that when the laser-induced breakdown spectroscopy (LIBS) technique is...
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- Application of one-point calibration LIBS for quantification of analytes
in samples with distinct matrix characteristics: a case study with Hg-
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Abstract: J. Anal. At. Spectrom., 2023, Accepted Manuscript
DOI : 10.1039/D2JA00399F, PaperLuis Carlos Leva Borduchi, Carlos Renato Menegatti, Débora Marcondes Bastos Pereira Milori, Hélcio José Izário Filho, Paulino Ribeiro Villas-Boas
Laser-induced breakdown spectroscopy (LIBS) is a powerful analytical technique for elemental analysis, but matrix effects can significantly affect its accuracy. In this work, we propose the use of calibration-free LIBS...
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