Please help us test our new pre-print finding feature by giving the pre-print link a rating. A 5 star rating indicates the linked pre-print has the exact same content as the published article.
Please help us test our new pre-print finding feature by giving the pre-print link a rating. A 5 star rating indicates the linked pre-print has the exact same content as the published article.
Please help us test our new pre-print finding feature by giving the pre-print link a rating. A 5 star rating indicates the linked pre-print has the exact same content as the published article.
Authors:Hua; Quan, Murray-Wallace, Colin V. Pages: 441 - 444 PubDate: 2025-05-07 DOI: 10.1017/RDC.2025.20
Please help us test our new pre-print finding feature by giving the pre-print link a rating. A 5 star rating indicates the linked pre-print has the exact same content as the published article.
Please help us test our new pre-print finding feature by giving the pre-print link a rating. A 5 star rating indicates the linked pre-print has the exact same content as the published article.
Authors:Beisel; E., Therre, S., Wienberg, C., Friedrich, R., Frank, N. Pages: 450 - 460 Abstract: Highly precise and reproducible radiocarbon (14C) measurements are regularly performed at the Heidelberg Institute for Environmental Physics, Heidelberg, Germany, in collaboration with the radiocarbon laboratory of the Curt-Engelhorn-Center Archaeometry in Mannheim, Germany. Here, we report an update of the technical details, focusing on the analysis of cold-water corals (CWC), and present an improved long-term blank value with a mean of (0.190 ± 0.064) pMC (n = 138) and excellent reproducibility of the IAEA-C2 standard with a mean of (41.15 ± 0.16) pMC (n = 75), consistent with its certified consensus value. Furthermore, 33 duplicates of the CWC 14C measurements agree within 2σ, 85% even within the 1σ range. This provides excellent conditions for accurate 14C measurements. As an application example, we present combined 230Th/U and 14C ages of a coral-bearing sediment core from the upper Mauritanian slope. The resulting ventilation age record confirms decreasing ventilation between 30 and 25 kyr BP, most likely reflecting a northward propagation of a water mass originating from the south. During the LGM, we confirm a previously hypothesized southward displacement of the Cap Verde Frontal Zone. With the onset of the deglaciation, our record documents again an advance of a southern-sourced water mass into the subtropical North Atlantic. During the Bølling-Allerød warm period, strong ventilation fluctuations possibly indicate temporal influence of southern-sourced water. PubDate: 2025-03-14 DOI: 10.1017/RDC.2025.7
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Authors:Bobrowski; P., Jórdeczka, M., Masojć, M., Gunchinsuren, B., Goslar, T., Sikora, R, Muntowski, P., Odsuren, D., Szmit, M., Bazargur, D., Michalec, G., Szykulski, J. Pages: 461 - 470 Abstract: We report a set of radiocarbon dating of prehistoric settlements located on the paleolake Baruun Khuree shores in the Gobi-Altai area, southern Mongolia. The obtained series of 11 AMS 14C measurements on charcoal and other charred plant macro-remains can be associated with one of the earliest episodes of the Holocene highly mobile desert-adapted hunter-gatherers activities from the Gobi desert (ca. 11,250–10,500 cal BP). Exploiting a wide range of environments, including dune fields, they are characterized by pottery usage and microblade core technology with wedge-shaped cores as well as osteological materials. These preliminary results are part of a project analyzing the nature of long-lasting prehistoric occupation around Tsakhiurtyn Hundi (Eng. Flint Valley)—one of the most extensive early prehistoric sites of Central Asia owing its name to the presence of abundant flint outcrops, lithic workshops and their innumerable flint artifacts. PubDate: 2025-03-27 DOI: 10.1017/RDC.2025.4
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Authors:Bolandini; Marco A., De Maria, Daniele, Haghipour, Negar, Wacker, Lukas, Hemingway, Jordon D., Eglinton, Timothy I., Bröder, Lisa Pages: 471 - 486 Abstract: By constraining organic carbon (OC) turnover times and ages, radiocarbon (14C) analysis has become a crucial tool to study the global carbon cycle. However, commonly used “bulk” measurements yield average turnover times, masking age variability within complex OC mixtures. One method to unravel intra-sample age distributions is ramped oxidation, in which OC is oxidized with the aid of oxygen at increasing temperatures. The resulting CO2 is collected over prescribed temperature ranges (thermal fractions) and analyzed for 14C content by accelerator mass spectrometry (AMS). However, all ramped oxidation instruments developed to date are operated in an “offline” configuration and require several manual preparation steps, hindering sample throughput and reproducibility. Here we describe a compact, online ramped oxidation (ORO) setup, where CO2 fractions are directly collected and transferred for 14C content measurement using an AMS equipped with a gas ion source. Our setup comprises two modules: (i) an ORO unit containing two sequential furnaces, the first of which holds the sample and is ramped from room temperature to ∼900°C, the second of which is maintained at 900°C and holds catalysts (copper oxide and silver) to ensure complete oxidation of evolved products to CO2; and (ii) a dual-trap interface (DTI) collection unit containing two parallel molecular sieve traps, which alternately collect CO2 from a given fraction and handle its direct injection into the AMS. Initial results for well-characterized samples indicate that 14C content uncertainties and blank background values are like those obtained during routine gas measurements at ETH, demonstrating the utility of the ORO-DTI setup. PubDate: 2025-04-04 DOI: 10.1017/RDC.2025.6
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Authors:DeLong; Kristine L., Kilbourne, K. Halimeda, Guilderson, Thomas P., Wagner, Amy J., Slowey, Niall, Palmer, Kylie, Hajdas, Irka Pages: 487 - 512 Abstract: Ocean radiocarbon (14C) is a proxy for air-sea exchange, vertical and horizontal mixing, and water mass identification. Here, we present five pre- to post-bomb coral Δ14C records from West Flower Garden Bank and Santiaguillo reefs in the Gulf of Mexico, Boca de Medio, and Isla Tortuga near the Cariaco Basin north of Venezuela. To assess basin-wide Δ14C variability, we compiled the Atlantic Ocean reef-building surface coral Δ14C records (24 corals and 28 data sets in total) with these new records. Cumulatively, the Δ14C records, on their independent age models, reveal the onset of post-bomb Δ14C trends in 1958 ±1 to 2 years. A general decrease in maximum Δ14C values occurs with decreasing latitude reflecting the balance between air-sea gas exchange and surface water residence time, vertical mixing, and horizontal advection. A slightly larger atmospheric imprint in the northern sites and relatively greater vertical mixing and/or advection of low-14C waters influence the southern Caribbean and eastern Atlantic sites. The eastern Atlantic sites, due to upwelling, have the lowest post-bomb Δ14C values. Equatorial currents from the eastern Atlantic transport low Δ14C water towards the western South Atlantic and southern Caribbean sites. Decadal Δ14C averages for the pre-bomb interval (1750–1949) for the low latitude western Atlantic are relatively constant within analytical (3–5‰) and chronological uncertainties (∼1–2 years) due to mixing and air-sea exchange. The compiled Δ14C records provide updated regional marine Δ14C values for marine reservoir corrections. PubDate: 2025-03-27 DOI: 10.1017/RDC.2025.5
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Authors:Gavranović; Mario, Webster, Lyndelle C., Kapuran, Aleksandar, Waltenberger, Lukas, Petschko, Irene M., Dević, Marina, Mittermair, Nicole Pages: 513 - 538 Abstract: Ever since the first discovery of urn burials in eastern Serbia during the 1980s, their dating has been uncertain and based on distant analogies and typological parallels. In this paper, we present radiocarbon dates from five urn cemeteries and three associated settlement sites, showing that the initial dating (Late Bronze Age; 14th–11th BCE) is highly questionable. Instead, radiocarbon dating and modeling presented here connect the urn cemeteries—characterized by a specific grave architecture and associated with settlements that display evidence of copper production—to a period between the 20th and 16th centuries BC. The fact that many of our dates come from cremated bones requires a discussion with regard to the circumstances of carbon exchange during cremation. The absolute dates thus far available for most urn cemeteries from the neighboring regions of the Balkans are all markedly younger (15th–11th century BC) than the data presented here and fall in the frame of the overall expansion of cremation in Europe during the Urnfield period. The new absolute dates from eastern Serbia provide a possibility to change our understanding of the Bronze Age dynamics of the 2nd millennium in the broader area of southeastern Europe and indicate a much earlier acceptance of cremation among certain groups than previously thought. PubDate: 2025-03-13 DOI: 10.1017/RDC.2025.8
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Authors:Göhring; Andrea, Hüls, C. Matthias, Hölzl, Stefan, Mayr, Christoph, Strauss, Harald, Hamann, Christian Pages: 539 - 564 Abstract: Marine aerosols can enter the terrestrial environment via sea spray which is known to affect the stable isotope fingerprint of coastal samples (plants, animals/humans), including δ13C. However, the impact of sea spray on 14C dating of terrestrial organisms at coastal sites has not been investigated so far. Besides a direct effect, sea spray is accompanied by physiological effects, e.g., due to salinity. In an artificial sea spray experiment in the greenhouse, the effect of sea spray on 14C in plant tissue was investigated. Beach grass was sprayed with mineral salt solutions containing only traces of NaCl or with brackish water from the Schlei inlet or the Baltic Sea. These plants should give a 14C signal close to the modern atmospheric 14CO2 composition. However, three treatment groups showed variable radiocarbon concentrations. Plants sprayed with water from the Schlei inlet, Baltic Sea water, or with a mineral salt solution with very high HCO3– concentration are depleted in 14C content relative to contemporary atmospheric composition. While δ13C reflects physiological effects in the plants, caused either by salinity (NaCl) or HCO3– stress, resulting in decreased discrimination against 13C, the uptake of high amounts of 14C (ca. 53–67%) from DIC (dissolved inorganic carbon) partly masks the underlying physiological reactions, as is visible in the radiocarbon signature of the plant tissues. This preliminary study indicates that sea spray effects on plant tissue could potentially influence faunal tissue 14C composition at coastal sites. Further research is required to better understand the observed reservoir effect. PubDate: 2025-02-20 DOI: 10.1017/RDC.2025.1
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Authors:Guan; Zuguang, Zhou, Yan, Ling, Qiang, Varricchio, Luca, Detti, Amelia, Bartalini, Saverio, Chen, Daru Pages: 565 - 577 Abstract: Radiocarbon (14C) measurements play important roles in dating and tracing applications where the isotopic concentration can differ from 0.1 to 106 pMC (percent modern carbon). A liquid scintillation counter cannot provide enough sensitivity when dealing with low-concentration samples of limited amounts over a reasonable time period. Accelerator mass spectroscopy (AMS) measures low-concentrations well but must first do dilution for high-concentration samples, and suffers from high instrument and maintenance costs. Saturated absorption CAvity Ring-down spectroscopy (SCAR) has now been developed into a practical technique with performances close to AMS but at much lower costs. The dynamic range covers 1–105 pMC, and the measurement uncertainties in the range of 0.4–1 pMC can be achieved within 0.5–2.5 hr of operation time. SCAR measures CO2 gases directly without graphitization in sample preparation. The typical sample consumption is ∼1 mg of carbon mass and the time for sample preparation can be as short as 15 min. Applications of SCAR to Suess-effect evaluation, biogenic-component analysis, ancient- and modern-sample dating, food-fraud detection and medicine-metabolism study have all been demonstrated by employing a close-to-automatic sample preparation system. PubDate: 2025-03-13 DOI: 10.1017/RDC.2025.10
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Authors:K; Arya Krishnan, S, Bharath, Sharma, Rajveer, Kumar, Pankaj, Chopra, Sundeep, T R, Reshmi, M, Sudheesh, N, Karunakara Pages: 578 - 599 Abstract: The application of a tube combustion system (pyrolyzer) for the batch combustion of low carbon content environmental matrices, such as soil and sediment, for determining 14C specific activity is examined. The samples were combusted at 600°C, and the CO2 species produced were trapped in 3N NaOH, precipitated as BaCO3 by adding BaCl2, and subjected to acid-hydrolysis to transfer the CO2 species to the absorber-scintillator mixture for liquid scintillation counting (LSC). The method was validated by analyzing the samples by accelerator mass spectrometry (AMS) method. The minimum detectable activity (MDA) for the method, at 2σ confidence level, was 10 Bq kg–1C (4 pMC) for a counting time of 500 min and 7 Bq kg–1C (3 pMC) for 1000 min. The capability of the method to quantify a small excess of 14C specific activity (a few Bq kg–1C or pMC) in the environment of a nuclear facility, when compared to the ambient natural background level, was demonstrated by analyzing a total of 23 soil and 7 sediment samples from the vicinity of a pressurized heavy water reactor (PHWR) nuclear power plant (NPP) at Kaiga, India. The maximum excess 14C specific activity values recorded for soil and sediment matrices were 37 ± 7 Bq kg–1C and 11 ± 7 Bq kg–1C, respectively, confirming minimal radioecological impact of the operation of the NPP on the environment. The 14C specific activity ratio for the recently fallen leaf litter and the soil underneath at most of the sampling points in the vicinity of the NPP had a mean value of 1.03 with an associated standard deviation of 0.07. Statistical tests confirm that the mean values of the data set of 14C specific activity of leaf litter and underlying soil are not significantly different. PubDate: 2025-05-08 DOI: 10.1017/RDC.2025.15
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Authors:Lindauer; Susanne, Händel, Marc, Magee, Peter Pages: 600 - 612 Abstract: We present reservoir effects on shells of species Terebralia palustris and Marcia spp. that were recovered during archaeological excavations at the multi-period site of Tell Abraq, Sharjah Emirate, UAE (This paper was presented at the combined 24th Radiocarbon and 10th Radiocarbon & Archaeology International Conference, Zurich, Switzerland, Sept. 2022.). The site was inhabited during the mid to late Holocene. It is situated in a lagoonal environment with former mangrove forests at the Arabian Gulf coast of southeast Arabia. Due to availability in the immediate proximity, shellfish played an important role for the local subsistence throughout the site’s occupation. Tell Abraq provides a well-defined and stratigraphically controlled archaeological context for investigations on the reservoir effect of the two species chosen. Crucial for the determination of the marine reservoir effect is comparison with contemporaneous terrestrial carbon samples. We discuss the data in a wider context with respect to results obtained at other sites. PubDate: 2025-05-19 DOI: 10.1017/RDC.2025.19
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Authors:Nielsen; Svein V., Hinz, Martin Pages: 613 - 629 Abstract: Marine flooding events occasionally interrupted the everyday lives of prehistoric coastal populations. Identification of such events are important for studies of past population dynamics and adaptive strategies. However, short-term events are rarely identified in the geological record, which puts a severe limit on our archaeological interpretive framework. This paper explores the temporality of the second Holocene transgression in southwestern Norway (ca. 3500 BCE) and works under the hypothesis that it was not a slow geological process but rather one or multiple short-term events. A Bayesian approach is used to analyze multidisciplinary time series data collected from sites located in Norway and Shetland. The resulting chronological model supports the hypothesis that the second Holocene transgression in southwestern Norway was a rapid flooding event that occurred in the period 3445–3395 BCE (Early Neolithic II). It is also suggested, but not argued conclusively, that this flooding event could correspond to the Garth tsunami, a paleotsunami named after Garth Loch in Shetland. Considering the potential impact of such a flooding event on the everyday lives of local foragers who dwelled in southwestern Norway, it is anticipated that this study could form a starting point for future case studies. PubDate: 2025-04-22 DOI: 10.1017/RDC.2025.14
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Authors:Regev; Dalit, Boaretto, Elisabetta, Gronau, Ilan Pages: 630 - 645 Abstract: In this paper, we examine cases where radiocarbon (14C) dates are incompatible with dates produced by other established archaeological methods. We present results from nine bones that we sampled from tombs in Phoenician sites in Sicily. These bones produced radiocarbon dates conflicting with established dates of finds in the associated tombs. These discrepancies, particularly in tomb dates, pose a serious problem, as they suggest that the finds may be disconnected from the buried individuals, challenging the fundamental premise of studying excavated tombs. To put our findings in a broader context, we also present other cases of discrepancies found in recent publications and note some common observations throughout these studies. Our questions and observations arise from the significant implications that radiocarbon dating has for our research on Phoenician ancient DNA, as these conflicts impact our understanding of the potential migration and movement of Phoenician people throughout the Mediterranean. PubDate: 2025-05-19 DOI: 10.1017/RDC.2025.17
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Authors:Scifo; Andrea, Dee, Michael Pages: 646 - 655 Abstract: Sudden annual rises in radiocarbon concentration have proven to be valuable assets for achieving exact-year calibration of radiocarbon measurements. These extremely precise calibrations have usually been obtained through the use of classical χ2 tests in conjunction with a local calibration curve of single-year resolution encompassing a rapid change in radiocarbon levels. As the latest Northern Hemisphere calibration curve, IntCal20, exhibits single-year resolution over the last 5000 years, in this study we investigate the possibility of performing calibration of radiocarbon dates using the classical χ2 test and achieving high-precision dating more extensively, examining scenarios without the aid of such abrupt changes in radiocarbon concentration. In order to perform a broad analysis, we simulated 171 sets of radiocarbon measurements over the last two millennia, with different set lengths and sample spacings, and tested the effectiveness of the χ2 test compared to the most commonly used Bayesian wiggle-matching technique for temporally ordered sequences of samples such as tree-rings sequences, the OxCal D_Sequence. The D_Sequence always produces a date range, albeit in certain cases very narrow; the χ2 test proves to be a viable alternative to Bayesian wiggle-matching, as it achieves calibrations of comparable precision, providing also a highest-likelihood estimate within the uncertainty range. PubDate: 2025-03-27 DOI: 10.1017/RDC.2025.9
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Authors:Kertész; Titanilla G., Hubay, Katalin, Buró, Botond, Jull, A. J. Timothy, Mindszenty, Andrea, Sipos, György, Bartyik, Tamás, Molnár, Mihály Pages: 656 - 678 Abstract: To investigate the environmental history of the Tisza River (Hungary), we applied 14C and OSL dating methods for five parallel, neighboring cores from the flood plain area (Jászság Basin). Four major sedimentary layers were identified: meadow soil on the top (S1); silty-clay (S2); clayey-silt (S3) section; and fine sand (S4). 14C and OSL data were integrated into a synthetic age-depth model using the BACON software package. Formation of the S1 layer (depth: 0–1.0 m) falls in the Holocene, up to 10 kyrs cal BP, with moderate sedimentation rate (100 yr/cm aAR). The S2 layer (1.0–8.0 m depth) represent the entire Last Glacial to Upper Pleniglacial period (19–27 kyrs cal BP), with a much faster sedimentation (20 yr/cm aAr). The S3 section (8.0–17.0 m) represents a longer period (27–45 kyrs cal BP) with similar sedimentation rate (19 yr/cm aAr) as S2. These clayey silt layers fall into the Late Pleistocene/Middle Pleniglacial period, a period of nearly 18 kyrs of sedimentation resulting ∼9 m thick sediment. Our study delivered some new and important details about the surface evolution of the investigated Tiszasüly area. A missing part of about 10 kyrs period (between 10–19 kyrs cal BP) was revealed in the investigated synthetic cores. PubDate: 2025-03-31 DOI: 10.1017/RDC.2024.140
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Authors:Kertész; Titanilla G., Gergely, Virág, Buró, Botond, Futó, István, Jull, A. J. Timothy, Molnár, Mihály Pages: 679 - 694 Abstract: Earthworm biospheroids are a useful alternative to radiocarbon (14C) soil dating. In this study, we undertook a series of measurements to test the 14C dating potential/performance of recent earthworm biospheroid granules. A novel sample preparation protocol for 14C in biospheroids was developed and elaborated at Atomki (Institute for Nuclear Research) and tested on IAEA reference materials. 24 natural biospheroid samples were extracted from five different location/environment-eight topsoils (A-horizon soils). Bomb-peak-based, high-resolution 14C dating show very uniform 14C results at 105.6 ± 2.6 pMC (1σ) and none of the biospheroids are older than 30 yr. It also shows that no biospheroid with a 14C bomb-peak as high as that observed in the 1960s and 1990s were observed. The results confirmed that earthworms do indeed consume almost exclusively recent biogenic carbon, not other organic compounds or inorganic carbonates previously bound in the soil. The calendar age of their biospheroids were extremely close to the real (zero) age of the surface. Thus, no “reservoir effect” is seen for these macrofossils. We conclude that a biospheroid-based 14C age determination method may be suitable to measure the burial time as long as earthworm biospheroids can be found in the soil. PubDate: 2025-03-14 DOI: 10.1017/RDC.2024.141
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Authors:Piotrowska; Natalia, Dreczko, Ewa, Fabiszak, Iga, Furmanek, Mirosław, Gomułka, Izabela, Hałuszko, Agata, Jarosz, Paweł, Józefowska-Domańska, Anna, Kamyszek, Lidia, Kołoszuk, Igor, Lasota-Kuś, Anna, Masojć, Mirosław, Minta-Tworzowska, Danuta, Murzyński, Tomasz, Pawełczyk, Fatima, Piekalski, Jerzy, Przybyła, Marcin M., Rychtarska, Marta, Sady-Bugajska, Agata, Szczepanek, Anita, Ustrzycka, Alicja, Żygadło, Leszek, Chmielewski, Tomasz J. Pages: 695 - 701 Abstract: This paper presents the results of accelerator mass spectrometry radiocarbon (AMS 14C) dating performed on archaeological samples (human bone, wood charcoal, and other charred plant macro-remains) from six sites located in the Lesser Poland Upland (southern Poland). We report 41 14C age measurements performed on discoveries made during the contract excavations carried out during the S7 roadway construction from 2016–2022. The resulting ages fall into a long interval, which, in terms of the regional archaeological periodization, lasts from the Late Neolithic to the Late Antiquity/Early Medieval Period (ca. 4600 BC–600 AD), and in terms of the climatological periodization corresponds to the Atlantic, Subboreal, and Subatlantic. PubDate: 2025-06-12 DOI: 10.1017/RDC.2025.21
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