Subjects -> METALLURGY (Total: 58 journals)
Showing 1 - 10 of 10 Journals sorted alphabetically
Acta Metallurgica Slovaca     Open Access   (Followers: 2)
Advanced Device Materials     Open Access   (Followers: 6)
American Journal of Fluid Dynamics     Open Access   (Followers: 44)
Archives of Metallurgy and Materials     Open Access   (Followers: 9)
Asian Journal of Materials Science     Open Access   (Followers: 4)
Canadian Metallurgical Quarterly     Hybrid Journal   (Followers: 21)
Complex Metals     Open Access   (Followers: 2)
Energy Materials : Materials Science and Engineering for Energy Systems     Hybrid Journal   (Followers: 24)
Graphene and 2D Materials     Open Access   (Followers: 6)
Handbook of Ferromagnetic Materials     Full-text available via subscription   (Followers: 1)
Handbook of Magnetic Materials     Full-text available via subscription   (Followers: 2)
High Temperature Materials and Processes     Open Access   (Followers: 6)
Indian Journal of Engineering and Materials Sciences (IJEMS)     Open Access   (Followers: 11)
International Journal of Metallurgy and Alloys     Full-text available via subscription   (Followers: 1)
International Journal of Metals     Open Access   (Followers: 7)
International Journal of Minerals, Metallurgy, and Materials     Hybrid Journal   (Followers: 11)
International Journal of Mining and Geo-Engineering     Open Access   (Followers: 4)
Ironmaking & Steelmaking     Hybrid Journal   (Followers: 5)
ISIJ International - Iron and Steel Institute of Japan     Full-text available via subscription   (Followers: 26)
Izvestiya Vuzov. Poroshkovaya Metallurgiya i Funktsional’nye Pokrytiya (Proceedings of Higher Schools. Powder Metallurgy аnd Functional Coatings)     Full-text available via subscription   (Followers: 2)
JOM Journal of the Minerals, Metals and Materials Society     Hybrid Journal   (Followers: 35)
Journal of Central South University     Hybrid Journal   (Followers: 1)
Journal of Cluster Science     Hybrid Journal  
Journal of Heavy Metal Toxicity and Diseases     Open Access  
Journal of Iron and Steel Research International     Hybrid Journal   (Followers: 11)
Journal of Materials & Metallurgical Engineering     Full-text available via subscription   (Followers: 2)
Journal of Materials Processing Technology     Hybrid Journal   (Followers: 21)
Journal of Metallurgical Engineering     Open Access   (Followers: 4)
Journal of Sustainable Metallurgy     Hybrid Journal   (Followers: 3)
Materials Science and Metallurgy Engineering     Open Access   (Followers: 6)
Metal Finishing     Full-text available via subscription   (Followers: 20)
Metallurgical and Materials Engineering     Open Access   (Followers: 7)
Metallurgical and Materials Transactions A     Hybrid Journal   (Followers: 41)
Metallurgical and Materials Transactions B     Hybrid Journal   (Followers: 32)
Metallurgical and Materials Transactions E     Full-text available via subscription   (Followers: 2)
Metallurgical Research and Technology     Full-text available via subscription   (Followers: 8)
Metallurgy and Foundry Engineering     Open Access   (Followers: 2)
Mining, Metallurgy & Exploration     Hybrid Journal  
Powder Diffraction     Full-text available via subscription   (Followers: 1)
Powder Metallurgy     Hybrid Journal   (Followers: 36)
Powder Metallurgy and Metal Ceramics     Hybrid Journal   (Followers: 8)
Powder Metallurgy Progress     Open Access   (Followers: 5)
Practical Metallography     Full-text available via subscription   (Followers: 6)
Rare Metals     Hybrid Journal   (Followers: 3)
Revista de Metalurgia     Open Access  
Revista del Instituto de Investigación de la Facultad de Ingeniería Geológica, Minera, Metalurgica y Geográfica     Open Access  
Revista Remetallica     Open Access   (Followers: 1)
Revue de Métallurgie     Full-text available via subscription  
Russian Metallurgy (Metally)     Full-text available via subscription   (Followers: 4)
Science and Technology of Welding and Joining     Hybrid Journal   (Followers: 7)
Steel Times lnternational     Partially Free   (Followers: 19)
Transactions of the IMF     Hybrid Journal   (Followers: 14)
Transactions of the Indian Institute of Metals     Hybrid Journal   (Followers: 5)
Tungsten     Hybrid Journal  
Universal Journal of Materials Science     Open Access   (Followers: 3)
Welding in the World     Hybrid Journal   (Followers: 7)
Welding International     Hybrid Journal   (Followers: 11)
Вісник Приазовського Державного Технічного Університету. Серія: Технічні науки     Open Access  
Similar Journals
Journal Cover
Powder Diffraction
Journal Prestige (SJR): 0.319
Citation Impact (citeScore): 1
Number of Followers: 1  
  Full-text available via subscription Subscription journal
ISSN (Print) 0885-7156 - ISSN (Online) 1945-7413
Published by Cambridge University Press Homepage  [395 journals]
  • PDJ volume 35 issue 4 Cover and Front matter
    • PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000706
      Issue No: Vol. 35, No. 4 (2020)
  • PDJ volume 35 issue 4 Cover and Back matter
    • PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000718
      Issue No: Vol. 35, No. 4 (2020)
  • Editorial
    • Authors: Camden Hubbard
      Pages: 225 - 225
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000676
      Issue No: Vol. 35, No. 4 (2020)
  • Quantification of solid-state impurity with powder X-ray diffraction using
           laboratory source
    • Authors: Meenakshi Sundaram; Saravanan Natarajan, Amol G. Dikundwar, Hemant Bhutani
      Pages: 226 - 232
      Abstract: The application of powder X-ray diffraction (PXRD) for the detection and quantification of low levels of a solid-state chemical impurity, BrettPhos oxide, in an active pharmaceutical ingredient is discussed. It is demonstrated that with appropriate methodology and experimentation, the impurity levels of as low as 0.07% w/w could be detected reliably and limit of quantification of 0.10% w/w could be achieved by PXRD, using a laboratory X-ray source. Method development, validation, and benchmarking using conventional high-performance liquid chromatography are presented in the manuscript highlighting the robustness and reproducibility of such measurements.
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000500
      Issue No: Vol. 35, No. 4 (2020)
  • in+situ+powder+X-ray+diffraction&rft.title=Powder+Diffraction&rft.issn=0885-7156&,+C.+Gelant,+D.+G.+Billing&rft_id=info:doi/10.1017/S0885715620000494">An investigation into the temperature phase transitions of synthesized
           lithium titanate materials doped with Al, Co, Ni and Mg by in situ powder
           X-ray diffraction
    • Authors: X. van Niekerk; E. E. Ferg, C. Gelant, D. G. Billing
      Pages: 233 - 246
      Abstract: Li4Ti5O12 (LTO) and its doped analogues Li4Ti4.95M0.05O12 (M = Al3+, Co3+, Ni2+, and Mg2+) were synthesized and characterized using in situ PXRD to monitor the phase transitions during the sol–gel synthesis of the spinel material. These results are complimented by thermogravimetric analysis, which illustrates the decomposition of the materials synthesized, where the final LTO products are seen to form at approximately 550 °C. The material has an amorphous structure from room temperature, coupled with a crystalline phase which is speculated to be H2Ti2O5·H2O. This crystalline phase disappears at 250 °C, with the material still in the amorphous state. The crystalline LTO phase starts at approximately 550 °C, with anatase co-crystallizing with the spinel phase. Rutile appears at 600 °C and co-crystallizes with the final product at 850 °C, where anatase is no longer seen. The rutile impurity remains present after cooling the material to room temperature, and results indicate that prolonged heating at 850 °C is required to reduce the rutile content. Rietveld refinement of diffraction patterns show that the unit-cell parameter increases with increasing temperature, coupled with a decrease when cooling the sample. The crystallite sizes follow the same trend, with a significant increase above temperatures of 750 °C.
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000494
      Issue No: Vol. 35, No. 4 (2020)
  • In+situ+XRPD+study+of+the+ambient-pressure+synthesis+of+nonstoichiometric+Ag3O+from+Ag–Ag2O+thin+films:+Phase+abundance,+unit-cell+parameters,+and+c/a+as+a+function+of+temperature+and+time&rft.title=Powder+Diffraction&rft.issn=0885-7156&,+David+Field,+Zachary+Wilson&rft_id=info:doi/10.1017/S0885715620000561">In situ XRPD study of the ambient-pressure synthesis of nonstoichiometric
           Ag3O from Ag–Ag2O thin films: Phase abundance, unit-cell parameters, and
           c/a as a function of temperature and time
    • Authors: Paul J. Schields; Nicholas Dunwoody, David Field, Zachary Wilson
      Pages: 247 - 261
      Abstract: Ag3O was synthesized by jet-milling magnetron-sputtered Ag–Ag2O thin films. Heating the jet-milled powders in air and N2 from 40 to 148 °C at ambient pressure produced Ag3O-rich powders. The phase composition and unit-cell parameters of the jet-milled powders were measured as a function of temperature with in situ X-ray powder diffraction experiments from −186 to 293 °C. Ag3O was also produced by ball milling and sonicating jet-milled films at ambient conditions. The phase composition, unit-cell parameters, and thermal-reaction rates indicate nonstoichiometric Ag3O was produced from the reaction of metastable, nonstoichiometric Ag2O (cuprite structure) and ccp Ag. The thermal expansion of Ag3O is anisotropic; below 25 °C, the a-axis expansion is about twice the c-axis expansion resulting in a negative slope of c/a(T). The reversal of the sign of c/a(T) near 25 °C is dramatic. The thermal reaction is arrested when the temperature is rapidly increased from ambient to 130 °C. Ag3O is metastable and decreases its unit-cell volume during kinetic decomposition to Ag when heated above ambient temperature in air and nitrogen. The relative volume expansion of Ag3O is about 80% less than Ag at room temperature and below. The suite of nonstoichiometric Ag3O produced by heating displays a linear relation between c/a and unit-cell volume at room temperature. The c/a and unit-cell volume of a hydrothermally grown Ag3O single crystal reported in a published structure determination was the Ag-rich, low-volume end member of the linear series. The c/a and unit-cell volume are sensitive indicators of the oxygen content and state of disorder.
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000561
      Issue No: Vol. 35, No. 4 (2020)
  • Validation of XRD phase quantification using semi-synthetic data
    • Authors: Nicola Döbelin
      Pages: 262 - 275
      Abstract: Validating phase quantification procedures of powder X-ray diffraction (XRD) data for an implementation in an ISO/IEC 17025 accredited environment has been challenging due to a general lack of suitable certified reference materials. The preparation of highly pure and crystalline reference materials and mixtures thereof may exceed the costs for a profitable and justifiable implementation. This study presents a method for the validation of XRD phase quantifications based on semi-synthetic datasets that reduces the effort for a full method validation drastically. Datasets of nearly pure reference substances are stripped of impurity signals and rescaled to 100% crystallinity, thus eliminating the need for the preparation of ultra-pure and -crystalline materials. The processed datasets are then combined numerically while preserving all sample- and instrument-characteristic features of the peak profile, thereby creating multi-phase diffraction patterns of precisely known composition. The number of compositions and repetitions is only limited by computational power and storage capacity. These datasets can be used as input files for the phase quantification procedure, in which statistical validation parameters such as precision, accuracy, linearity, and limits of detection and quantification can be determined from a statistically sound number of datasets and compositions.
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000573
      Issue No: Vol. 35, No. 4 (2020)
  • 1−xSex+nanobelts&rft.title=Powder+Diffraction&rft.issn=0885-7156&,+Bingsheng+Du,+Junhao+Ma,+Peihua+Wang,+Jikang+Jian&rft_id=info:doi/10.1017/S0885715620000615">Synthesis and optical properties of single-crystalline SnS1−xSex
    • Authors: Shengru Wang; Xiaofang Lai, Bingsheng Du, Junhao Ma, Peihua Wang, Jikang Jian
      Pages: 276 - 281
      Abstract: In this work, SnS1−xSex ternary nanobelts were synthesized by a facile hydrothermal method without the assistance of surfactants. The structure, morphology, microstructure, compositions, chemical valences, phonon modes, and optical band gaps of the SnS1−xSex nanobelts were characterized in detail. The results indicate that the SnS1−xSex nanobelts have uniform one-dimensional morphology and are single crystals with high crystallinity. Se is incorporated into the SnS lattice to substitute for S-forming ternary SnS1−xSex alloy. With the increase of Se doping concentration, the optical band gaps of the nanobelts gradually decrease from 1.15 to 1.01 eV, confirming the tunable optical property achieved here.
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000615
      Issue No: Vol. 35, No. 4 (2020)
  • 18H22O2&rft.title=Powder+Diffraction&rft.issn=0885-7156&,+Xiaoyan+Bian,+Qing+Wang&rft_id=info:doi/10.1017/S0885715620000512">X-ray powder diffraction data for estra-4,9-diene-3,17-dione, C18H22O2
    • Authors: Zhicheng Zha; Ting Tang, Xiaoyan Bian, Qing Wang
      Pages: 282 - 285
      Abstract: X-ray powder diffraction data for estra-4,9-diene-3,17-dione, C18H22O2, are reported [a = 9.236(7) Å, b = 10.294(4) Å, c = 15.471(1) Å, unit cell volume V = 1471.11 Å3, Z = 4, and space group P212121]. All measured lines were indexed and are consistent with the P212121 space group. No detectable impurities were observed. The single-crystallographic data of the compound are also reported [a = 9.2392(7) Å, b = 10.2793(5) Å, c = 15.4822(7) Å, unit cell volume V = 1470.37(15) Å3, Z = 4, and space group P212121]. Both single-crystal and powder diffraction methods can get the similar structure data.
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000512
      Issue No: Vol. 35, No. 4 (2020)
  • 17H24NO3)2(SO4)(H2O)&rft.title=Powder+Diffraction&rft.issn=0885-7156&,+Thomas+N.+Blanton&rft_id=info:doi/10.1017/S0885715620000603">Crystal structure of hyoscyamine sulfate monohydrate,
    • Authors: James A. Kaduk; Amy M. Gindhart, Thomas N. Blanton
      Pages: 286 - 292
      Abstract: The crystal structure of hyoscyamine sulfate monohydrate has been solved and refined using synchrotron X-ray powder diffraction data and optimized using density functional techniques. Hyoscyamine sulfate monohydrate crystallizes in space group P21 (#4) with a = 6.60196(2), b = 12.95496(3), c = 20.93090(8) Å, β = 94.8839(2)°, V = 1783.680(5) Å3, and Z = 2. Despite the traditional description as a dihydrate, hyoscyamine sulfate crystallizes as a monohydrate. The two independent hyoscyamine cations have different conformations, which have similar energies. One of the cations is close to the minimum-energy conformation. Each of the protonated nitrogen atoms in the cations acts as a donor to the sulfate anion. The hydroxyl group of one cation acts as a donor to the sulfate anion, while the hydroxyl group of the other cation acts as a donor to the water molecule. The water molecule acts as a donor to two different sulfate anions. The cations and anions are linked by complex chains of hydrogen bonds along the a-axis. The powder pattern has been submitted for inclusion in the Powder Diffraction File™ (PDF®).
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000603
      Issue No: Vol. 35, No. 4 (2020)
  • 16H17N3O4S(H2O)&rft.title=Powder+Diffraction&rft.issn=0885-7156&,+Thomas+N.+Blanton&rft_id=info:doi/10.1017/S0885715620000627">Crystal structure of cephalexin monohydrate, C16H17N3O4S(H2O)
    • Authors: James A. Kaduk; Amy M. Gindhart, Thomas N. Blanton
      Pages: 293 - 300
      Abstract: The crystal structure of cephalexin monohydrate has been solved and refined using synchrotron X-ray powder diffraction data and optimized using density functional techniques. Cephalexin monohydrate crystallizes in space group C2 (#5) with a = 27.32290(17), b = 11.92850(4), c = 16.75355(8) Å, β = 108.8661(4)°, V = 5166.99(3) Å3, and Z = 12. Although the general arrangement of molecules is similar to that in cephalexin dihydrate, the structural differences result in very different powder patterns. The crystal structure is characterized by alternating layers of hydrogen bonds and van der Waals contacts parallel to the bc-plane. The water molecules occur in clusters. Five of the six protons in the water molecules act as donors in O–H⋯O hydrogen bonds. The sixth hydrogen atom acts as a donor to two different phenyl ring carbon atoms to form bifurcated O–H⋯C hydrogen bonds. Each cephalexin molecule is a zwitterion, containing ammonium and carboxylate groups. The ammonium ions form N–H⋯O hydrogen bonds to carboxylate groups and water molecules, as well as to carbonyl groups. The powder pattern is included in the Powder Diffraction File™ as entry 00-065-1417.
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000627
      Issue No: Vol. 35, No. 4 (2020)
  • Calendar of Short Courses and Workshops
    • Authors: Gang Wang
      Pages: 301 - 301
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000585
      Issue No: Vol. 35, No. 4 (2020)
  • Calendar of Forthcoming Meetings
    • Authors: Gang Wang
      Pages: 302 - 303
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000597
      Issue No: Vol. 35, No. 4 (2020)
  • 69th Annual Denver X-ray conference report – a virtual event!
    • Authors: Denise Zulli
      Pages: 304 - 306
      PubDate: 2020-12-01T00:00:00.000Z
      DOI: 10.1017/S0885715620000652
      Issue No: Vol. 35, No. 4 (2020)
School of Mathematical and Computer Sciences
Heriot-Watt University
Edinburgh, EH14 4AS, UK
Tel: +00 44 (0)131 4513762

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