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Chemical Science
Journal Prestige (SJR): 4.508  Citation Impact (citeScore): 9 Number of Followers: 24  Open Access journalISSN (Print) 1478-6524 - ISSN (Online) 2041-6520 Published by RSC  [43 journals]
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- Folding mechanisms steer the amyloid fibril formation propensity of highly
homologous proteins
Pages: 3290 - 3298
Abstract:Chem. Sci. , 2018, 9 ,3290-3298
DOI : 10.1039/C8SC00166A, Edge Article
Open Access 
This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Gaetano Malgieri, Gianluca D'Abrosca, Luciano Pirone, Angelo Toto, Maddalena Palmieri, Luigi Russo, Michele Francesco Maria Sciacca, Rosarita Tate, Valeria Sivo, Ilaria Baglivo, Roksana Majewska, Massimo Coletta, Paolo Vincenzo Pedone, Carla Isernia, Mario De Stefano, Stefano Gianni, Emilia Maria Pedone, Danilo Milardi, Roberto Fattorusso
Understanding the molecular determinants of fibrillogenesis by studying the aggregation propensities of high homologous proteins with different folding pathways.
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Issue No: Vol. 9 (2018)
- In operando imaging of self-catalyzed formaldehyde burst in methanol
oxidation reactions under open circuit conditions
Pages: 3318 - 3323
Abstract:Chem. Sci. , 2018, 9 ,3318-3323
DOI : 10.1039/C7SC05347A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Liang Yuan, Meng Li, Tinglian Yuan, Yimin Fang, Wei Wang
A wave-like HCHO burst is in situ observed during electro-oxidation of methanol on Pt under open circuit conditions by SPR imaging.
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Issue No: Vol. 9 (2018)
- Step-growth titanium-catalysed dehydropolymerisation of amine-boranes
Pages: 3360 - 3366
Abstract:Chem. Sci. , 2018, 9 ,3360-3366
DOI : 10.1039/C7SC05395A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Titel Jurca, Theresa Dellermann, Naomi E. Stubbs, Diego A. Resendiz-Lara, George R. Whittell, Ian Manners
Titanium-catalysed dehydropolymerisation of primary amine-boranes was found to proceed via a step-growth rather than a chain-growth mechanism.
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Issue No: Vol. 9 (2018)
- Computational evaluation of metal pentazolate frameworks: inorganic
analogues of azolate metal-organic frameworks
Pages: 3367 - 3375
Abstract:Chem. Sci. , 2018, 9 ,3367-3375
DOI : 10.1039/C7SC05020H, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Mihails Arhangelskis, Athanassios D. Katsenis, Andrew J. Morris, Tomislav Friscic
We report a periodic density-functional theory evaluation of putative frameworks, including a topologically novel arhangelskite ( arh ) structure, based on the pentazolate ion, the ultimate all-nitrogen, inorganic member of the azolate series of aromatic 5-membered ring anions.
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Issue No: Vol. 9 (2018)
- Tailored metastable Ce-Zr oxides with highly distorted lattice oxygen for
accelerating redox cycles
Pages: 3386 - 3394
Abstract:Chem. Sci. , 2018, 9 ,3386-3394
DOI : 10.1039/C8SC00729B, Edge Article Open Access 
This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Zhe Zhang, Jiafeng Yu, Jixin Zhang, Qingjie Ge, Hengyong Xu, Felix Dallmann, Roland Dittmeyer, Jian Sun
Oxygen release in redox cycles is enhanced due to the formation of disordered lattice oxygen in the quenching process.
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Issue No: Vol. 9 (2018)
- Stable 2D anti-ferromagnetically coupled fluorenyl radical dendrons
Pages: 3395 - 3400
Abstract:Chem. Sci. , 2018, 9 ,3395-3400
DOI : 10.1039/C7SC05493A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Jian Wang, Gakhyun Kim, Maria Eugenia Sandoval-Salinas, Hoa Phan, Tullimilli Y. Gopalakrishna, Xuefeng Lu, David Casanova, Dongho Kim, Jishan Wu
The first class of stable two-dimensional anti-ferromagnetically coupled dendritic polyradicaloids was synthesized, which show polyradical character and unique properties.
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Issue No: Vol. 9 (2018)
- Lanthanide doping induced electrochemical enhancement of Na2Ti3O7 anodes
for sodium-ion batteries
Pages: 3421 - 3425
Abstract:Chem. Sci. , 2018, 9 ,3421-3425
DOI : 10.1039/C7SC05185A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Jiale Xia, Hongyang Zhao, Wei Kong Pang, Zongyou Yin, Bo Zhou, Gang He, Zaiping Guo, Yaping Du
Lanthanide doped Na 2 Ti 3 O 7 enabled remarkably higher capacity for sodium ion batteries due to the enhanced conductivity by introducing oxygen vacancies.
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Issue No: Vol. 9 (2018)
- On the role of Ce in CO2 adsorption and activation over lanthanum species
Pages: 3426 - 3437
Abstract:Chem. Sci. , 2018, 9 ,3426-3437
DOI : 10.1039/C8SC00203G, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Xinyu Li, Zhi-Jian Zhao, Liang Zeng, Jiubing Zhao, Hao Tian, Sai Chen, Kang Li, Sier Sang, Jinlong Gong
This paper describes the influence of Ce addition on the CO 2 adsorption and activation over La 2 O 3 . Ce addition is verified to promote the formation of bidentate carbonate on La 2 O 3 and affect the ratio of hexagonal/monoclinic La 2 O 2 CO 3 on the Ce-La binary oxides.
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Issue No: Vol. 9 (2018)
- Understanding the charge transport properties of redox active
metal-organic conjugated wires
Pages: 3438 - 3450
Abstract:Chem. Sci. , 2018, 9 ,3438-3450
DOI : 10.1039/C7SC04727D, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Donglei Bu, Yingqi Xiong, Ying Ning Tan, Miao Meng, Paul J. Low, Dai-Bin Kuang, Chun Y. Liu
For Rh 2 -organic molecular wires, we found that weaker coupling systems built using longer bridging ligands exhibit better electrical conductance.
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Issue No: Vol. 9 (2018)
- A promising bulky anion based lithium borate salt for lithium metal
batteries
Pages: 3451 - 3458
Abstract:Chem. Sci. , 2018, 9 ,3451-3458
DOI : 10.1039/C8SC00041G, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Lixin Qiao, Zili Cui, Bingbing Chen, Gaojie Xu, Zhonghua Zhang, Jun Ma, Huiping Du, Xiaochen Liu, Suqi Huang, Kun Tang, Shanmu Dong, Xinhong Zhou, Guanglei Cui
A promising lithium borate salt for next generation lithium metal batteries.
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Issue No: Vol. 9 (2018)
- Development of microfluidic platforms for the synthesis of metal complexes
and evaluation of their DNA affinity using online FRET melting assays
Pages: 3459 - 3469
Abstract:Chem. Sci. , 2018, 9 ,3459-3469
DOI : 10.1039/C8SC00528A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Viktoria Rakers, Paolo Cadinu, Joshua B. Edel, Ramon Vilar
Two new microfluidic platforms are reported to synthesize metal complexes and assess their DNA affinity in continuous flow.
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Issue No: Vol. 9 (2018)
- Trends in activity for the oxygen evolution reaction on transition metal
(M = Fe, Co, Ni) phosphide pre-catalysts
Pages: 3470 - 3476
Abstract:Chem. Sci. , 2018, 9 ,3470-3476
DOI : 10.1039/C7SC05033J, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Junyuan Xu, Junjie Li, Dehua Xiong, Bingsen Zhang, Yuefeng Liu, Kuang-Hsu Wu, Isilda Amorim, Wei Li, Lifeng Liu
A notable trend in OER activity on transition metal phosphide pre-catalysts is reported. Remarkably, the tri-metallic FeCoNiP pre-catalysts exhibit exceptional apparent and intrinsic OER activities, outperforming many non-precious OER catalysts reported previously.
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Issue No: Vol. 9 (2018)
- Donor-acceptor interactions between cyclic trinuclear pyridinate
gold(I)-complexes and electron-poor guests: nature and energetics of
guest-binding and templating on graphite
Pages: 3477 - 3483
Abstract:Chem. Sci. , 2018, 9 ,3477-3483
DOI : 10.1039/C7SC05355J, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Raiko Hahn, Fabian Bohle, Stefan Kotte, Tristan J. Keller, Stefan-S. Jester, Andreas Hansen, Stefan Grimme, Birgit Esser
Aromatic stacking interactions of [small pi]-basic Au( I ) complexes with [small pi]-acids were analyzed experimentally, theoretically and at the solid/liquid interface using STM.
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Issue No: Vol. 9 (2018)
- Enantiocontrol by assembled attractive interactions in copper-catalyzed
asymmetric direct alkynylation of [small alpha]-ketoesters with terminal
alkynes: OH[three dots, centered]O/sp3-CH[three dots, centered]O two-point
hydrogen bonding combined with dispersive attractions
Pages: 3484 - 3493
Abstract:Chem. Sci. , 2018, 9 ,3484-3493
DOI : 10.1039/C8SC00527C, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Martin C. Schwarzer, Akane Fujioka, Takaoki Ishii, Hirohisa Ohmiya, Seiji Mori, Masaya Sawamura
A chiral copper catalyst selects enantiofaces by assembled attractive interactions.
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Issue No: Vol. 9 (2018)
- Pentacyclic adenine: a versatile and exceptionally bright fluorescent DNA
base analogue
Pages: 3494 - 3502
Abstract:Chem. Sci. , 2018, 9 ,3494-3502
DOI : 10.1039/C7SC05448C, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Mattias Bood, Anders F. Fuchtbauer, Moa S. Wranne, Jong Jin Ro, Sangamesh Sarangamath, Afaf H. El-Sagheer, Deborah L. M. Rupert, Rachel S. Fisher, Steven W. Magennis, Anita C. Jones, Fredrik Hook, Tom Brown, Byeang Hyean Kim, Anders Dahlen, L. Marcus Wilhelmsson, Morten Grotli
A highly fluorescent, non-perturbing, pentacyclic adenine analog was designed, synthesized, incorporated into DNA and photophysical evaluated.
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Issue No: Vol. 9 (2018)
- On-chip measurements of protein unfolding from direct observations of
micron-scale diffusion
Pages: 3503 - 3507
Abstract:Chem. Sci. , 2018, 9 ,3503-3507
DOI : 10.1039/C7SC04331G, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yuewen Zhang, Emma[space]V. Yates, Liu Hong, Kadi L. Saar, Georg Meisl, Christopher M. Dobson, Tuomas P. J. Knowles
The unfolding process of BSA in solution as a function of pH was studied by microfluidic diffusional sizing device.
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Issue No: Vol. 9 (2018)
- Linking defects, hierarchical porosity generation and desalination
performance in metal-organic frameworks
Pages: 3508 - 3516
Abstract:Chem. Sci. , 2018, 9 ,3508-3516
DOI : 10.1039/C7SC05175A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Weibin Liang, Lin Li, Jingwei Hou, Nicholas D. Shepherd, Thomas D. Bennett, Deanna M. D'Alessandro, Vicki Chen
The composite membranes with defective metal-organic frameworks (MOFs) show a significant increase in water flux, without compromising the high salt rejection.
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Issue No: Vol. 9 (2018)
- An exploration of nucleic acid liquid biopsy using a glucose meter
Pages: 3517 - 3522
Abstract:Chem. Sci. , 2018, 9 ,3517-3522
DOI : 10.1039/C8SC00627J, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yu Gu, Ting-Ting Zhang, Zhi-Feng Huang, Shan-Wen Hu, Wei Zhao, Jing-Juan Xu, Hong-Yuan Chen
A proof-of-concept strategy for a circulating miRNA assay using a personal glucose meter (PGM) was proposed.
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Issue No: Vol. 9 (2018)
- Porous aromatic framework with mesopores as a platform for a
super-efficient heterogeneous Pd-based organometallic catalysis
Pages: 3523 - 3530
Abstract:Chem. Sci. , 2018, 9 ,3523-3530
DOI : 10.1039/C8SC00510A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Li-Ping Jing, Jin-Shi Sun, Fuxing Sun, Peng Chen, Guangshan Zhu
A porous aromatic framework with mesopores was used as a platform for an immobilized Pd catalyst with superb catalytic activity and size selectivity for the Suzuki-Miyaura coupling reaction.
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Issue No: Vol. 9 (2018)
- Exploiting the interactions between the ruthenium Hoveyda-Grubbs catalyst
and Al-modified mesoporous silica: the case of SBA15 vs. KCC-1
Pages: 3531 - 3537
Abstract:Chem. Sci. , 2018, 9 ,3531-3537
DOI : 10.1039/C7SC05200F, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Baraa Werghi, Eva Pump, Mykyta Tretiakov, Edy Abou-Hamad, Andrei Gurinov, Pradeep Doggali, Dalaver H. Anjum, Luigi Cavallo, Anissa Bendjeriou-Sedjerari, Jean-Marie Basset
2 nd generation Hoveyda-Grubbs catalyst immobilized onto well-ordered 2D hexagonal (SBA15) and 3D fibrous (KCC-1) mesostructured silica displaying tetra-coordinated Al-H via Surface Organometallic Chemistry (SOMC).
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Issue No: Vol. 9 (2018)
- Unexpected solvation-stabilisation of ions in a protic ionic liquid:
insights disclosed by a bond energetic study
Pages: 3538 - 3543
Abstract:Chem. Sci. , 2018, 9 ,3538-3543
DOI : 10.1039/C7SC05227H, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Zhen Wang, Feixiang Gao, Pengju Ji, Jin-Pei Cheng
Accurate acidity studies of different families of substrates in a pure protic ionic liquid (PIL) show that solute ions in the PIL are free from specific ion associations and the solvation behaviour of PILs is closely related to the number of dissociable protons.
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Issue No: Vol. 9 (2018)
- Glucose-nucleobase pairs within DNA: impact of hydrophobicity, alternative
linking unit and DNA polymerase nucleotide insertion studies
Pages: 3544 - 3554
Abstract:Chem. Sci. , 2018, 9 ,3544-3554
DOI : 10.1039/C7SC04850E, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Empar Vengut-Climent, Pablo Penalver, Ricardo Lucas, Irene Gomez-Pinto, Anna Avino, Alicia M. Muro-Pastor, Elsa Galbis, M. Violante de Paz, Celia Fonseca Guerra, F. Matthias Bickelhaupt, Ramon Eritja, Carlos Gonzalez, Juan Carlos Morales
Glucose-nucleobase pairs were designed, synthesized and incorporated into duplex DNA. Their stability, structure and polymerase replication was investigated.
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Issue No: Vol. 9 (2018)
- Highly active nano-sized iridium catalysts: synthesis and operando
spectroscopy in a proton exchange membrane electrolyzer
Pages: 3570 - 3579
Abstract:Chem. Sci. , 2018, 9 ,3570-3579
DOI : 10.1039/C8SC00555A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. P. Lettenmeier, J. Majchel, L. Wang, V. A. Saveleva, S. Zafeiratos, E. R. Savinova, J.-J. Gallet, F. Bournel, A. S. Gago, K. A. Friedrich
Ultra-high purity nano-sized iridium enclosed in a monolayer of Ir III /Ir IV oxides/hydroxides leads to an enhancement in OER activity.
The content of this RSS Feed (c) The Royal Society of Chemistry
Issue No: Vol. 9 (2018)
- Graftable SCoMPIs enable the labeling and X-Ray fluorescence imaging of
proteins
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00886H, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Sarah Hostachy, Marie Masuda, Takayuki Miki, Itaru Hamachi, Sandrine Sagan, Olivier LEQUIN, Kadda Medjoubi, Andrea SOMOGYI, Nicolas Delsuc, Clotilde Policar
Bio-imaging techniques alternative to fluorescence microscopy are gaining increasing interest as com-plementary tools to visualize and interrogate biolog-ical systems. Among them, X-ray fluorescence mi-crospectroscopy provides information on the local content...
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- Taming Monomeric [Cu([small eta]6-C6H6)]+ Complex with Silylene
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00459E, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Nasrina Parvin, Shiv Pal, Jorge Echeverria, Santiago Alvarez, Shabana Khan
Previous theoretical and experimental endeavors suggested that [Cu(C6H6)]+ prefers [small eta]1/[small eta]2 mode over [small eta]6 mode due to the augmented repulsion between the benzene ring and metal d-electrons. Nevertheless, the use of...
The content of this RSS Feed (c) The Royal Society of Chemistry
- Pd Nanosheets with Surface Coordinated by Radioactive Iodide as a
High-Performance Theranostic Nanoagent for Orthotopic Hepatocellular
Carcinoma Imaging and Cancer Therapy
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00104A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Mei Chen, Zhide Guo, Qinghua Chen, Jingping Wei, Jingchao Li, Changrong Shi, Duo Xu, Dawang Zhou, Xianzhong Zhang, Nanfeng Zheng
Radiolabeled nanoparticles (NPs), taking advantages of nanotechnology and nuclear medicine, have shown attractive potential for cancer diagnosis and therapy. However, high background signal in liver and long-time toxic effects of...
The content of this RSS Feed (c) The Royal Society of Chemistry
- Integration of isothermal amplification with quantum dot-based
fluorescence resonance energy transfer for simultaneous detection of
multiple microRNAs
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00832A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Juan Hu, Ming-hao Liu, Chun-yang Zhang
MicroRNAs (miRNAs) are small non-coding RNAs that regulate important physiological processes, and their dysregulation is associated with various human diseases. Simultaneously sensitive detection of multiple miRNAs may facilitate the early...
The content of this RSS Feed (c) The Royal Society of Chemistry
- Towards a molecular understanding of cellulose dissolution in ionic
liquids: anion/cation effect, synergistic mechanism and physicochemical
aspects
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C7SC05392D, Perspective Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yao Li, Jianji Wang, Xiaomin Liu, Suojiang Zhang
This perspective summarizes mechanistic studies on cellulose dissolution in ionic liquids, highlighting the synergistic mechanism, physicochemical aspects and future research trends.
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- A Porous, Electrically Conductive Hexa-Zirconium(IV) Metal-Organic
Framework
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00961A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Subhadip Goswami, Debmalya Ray, Ken-ichi Otake, Chung-Wei Kung, Sergio J Garibay, Timur Islamoglu, Ahmet Atilgan, Yuexing Cui, Christopher J. Cramer, Omar K. Farha, J T Hupp
Engendering electrical conductivity in high-porosity metal-organic frameworks (MOFs) promises to unlock the full potential of MOFs for electrical energy storage, electrocatalysis, or integration of MOFs with conventional electronic materials. Here...
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- Flying MOFs: Polyamine-containing fluidized MOF/SiO2 hybrid materials for
CO2 capture from post-combustion flue gas
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05372J, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Ignacio Luz Minguez, Mustapha Soukri, Marty A. Lail
Solid-state synthesis ensures a high loading and well-dispersed growth of a large collection of metal-organic framework (MOF) nanostructures within a series of commercially available mesoporous silica. This approach provides a...
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- Protecting Group Free Radical C-H Trifluoromethylation of Peptides
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00368H, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Naoko Ichiishi, John Caldwell, Melissa Lin, Wendy Zhong, Xiaohong Zhu, Eric C. Streckfuss, Hai-Young Kim, Craig A. Parish, Shane Krska
Two radical-based approaches have been developed to effect the trifluoromethylation of aryl C-H bonds in native peptides either using stoichiometric oxidant or visible light photoredox catalysis. The reported methods are...
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- Origin of Poor Doping Efficiency in Solution Processed Organic
Semiconductors
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00758F, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Ajay Jha, Hong-Guang Duan, Vandana Tiwari, Michael Thorwart, R.J. Dwayne Miller
Doping is an extremely important process where intentional insertion of impurities in semiconductors controls their electronic properties. In organic semiconductors, one of the convenient, but inefficient, ways of doping is...
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- Unusual mechanisms in Claisen rearrangements: an ionic fragmentation
leading to a meta-selective rearrangement
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C7SC04736C, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Boris Maryasin, Dainis Kaldre, Renan Galaverna, Immo Klose, Stefan Ruider, Martina Drescher, Hanspeter Kahlig, Leticia Gonzalez, Marcos N. Eberlin, Igor D. Jurberg, Nuno Maulide
A mechanistic investigation of the acid-catalysed redox-neutral arylation of ynamides intertwining ESI-MS, DFT and experiments reveals diverse pathways available from an otherwise simple-looking transformation.
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- DNA-binding miniproteins based on zinc fingers. Assessment of the
interaction using nanopores
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C7SC05441F, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Jessica Rodriguez, Soraya Learte-Aymami, Jesus Mosquera, Garbine Celaya, David Rodriguez-Larrea, M. Eugenio Vazquez, Jose L. Mascarenas
We report a synthetic miniprotein that combines zinc finger modules of the transcription factor GAGA with the AT-hook peptide. This designed chimera binds to extended DNA sites with high affinity and selectivity, as shown by nanopore force spectroscopy.
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- The cycloaspeptides: uncovering a new model for methylated nonribosomal
peptide biosynthesis
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00717A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Kate[space]M. J. de Mattos-Shipley, Claudio Greco, David M. Heard, Gemma Hough, Nicholas P. Mulholland, Jason L. Vincent, Jason Micklefield, Thomas J. Simpson, Christine L. Willis, Russell J. Cox, Andrew M. Bailey
The cycloaspeptide gene cluster includes a pathway-specific N -methyl transferase. Its disruption allowed incorporation of N -methylated amino acids provided in the culture medium, allowing efficient production of cycloaspeptide E and novel related products.
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- Electrochemical Imaging of Cells and Tissues
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC01035H, Minireview Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Tzu-En Lin, Stefania Rapino, Hubert Girault, Andreas Lesch
The technological and experimental progress in electrochemical imaging of biological specimens is discussed with a view on potential applications for skin cancer diagnostics, reproductive medicine and microbial testing. The electrochemical...
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- Iron-catalyzed urea synthesis: dehydrogenative coupling of methanol and
amines
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00775F, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Elizabeth[space]M. Lane, Nilay Hazari, Wesley H. Bernskoetter
An iron catalyzed method for selective urea synthesis is described. This approach couples methanol and amines to generate diverse organic ureas.
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- Why One Can Expect Large Rectification in Molecular Junctions Based on
Alkane Monothiols and Why Rectification Is So Modest
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00938D, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Zuoti Xie, Ioan Baldea, C Daniel Frisbie
Many attempts to obtain high current rectification ratios (RR) in molecular electronics are triggered by a potentiometer rule argument, which predicts that a strongly asymmetric location of the dominant molecular...
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- 9,10-Azaboraphenanthrene-Containing Small Molecules and Conjugated
Polymers: Synthesis and Their Application in Chemodosimeters for the
Ratiometric Detection of Fluoride Ions
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00688A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Wei-Dong Zhang, Guoping Li, Letian Xu, Yue Zhuo, Wen-Ming Wan, Ni Yan, Gang He
The introduction of main group elements into conjugated scaffold is emerging as a key route to novel optoelectronic materials. Herein, an efficient and versatile way to synthesize polymerizable 9,10-azaboraphenanthrene (BNP)-containing...
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- Composition-adjustable Ag-Au substitutional alloy microcages enabling
tunable plasmon resonance for ultrasensitive SERS
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00915E, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Xiaotian Wang, Guanshui Ma, Anran Li, Jian Yu, Zhao Yang, Jie Lin, Ang Li, Xiaodong Han, Lin Guo
A facile NaBH 4 -cooperative GRR strategy generating composition-adjustable Ag-Au substitutional alloy microcages enabling tunable plasmon resonance for ultrasensitive SERS.
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- Aldehyde group driven aggregation-induced enhanced emission in
naphthalimides and its application for ultradetection of hydrazine on
multiple platforms
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00643A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Niranjan Meher, Swagatika Panda, Sachin Kumar, Parameswar Krishnan Iyer
A new concept of formyl group induced ACQ to AIEE transformation is established in naphthalimide congeners. Also, ultradetection of hydrazine via Schiff base complexation over multiple platforms is presented.
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- A Thioether-directed Palladium-cleavable Linker for Targeted Bioorthogonal
Drug Decaging
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00256H, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Benjamin Stenton, Bruno Oliveira, Maria Matos, Laura Sinatra, Goncalo J. L. Bernardes
We describe the development of a bifunctional linker that simultaneously allows site-specific protein modification and palladium-mediated bioorthogonal decaging. This was enabled by a thioether binding motif in the propargyl carbamate...
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- Nontrigonal Constraint Enhances 1,2-Addition Reactivity of Phosphazenes
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00929E, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yi-Chun Lin, James Connor Gilhula, Alexander Radosevich
The syntheses and 1,2-addition reactivities of nontrigonal phosphazenes supported by trianionic tricoordinating chelates of the type L3P=Ndipp (3: L3 = N[CHC(tBu)O] 2 3-; 4: L3 = N(o-NMeC6H4) 2 3-; dipp = 2,6-diisopropylphenyl) are reported....
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- Diastereoisomers of L-Proline-linked trityl-nitroxide biradicals:
synthesis and effect of chiral configurations on exchange interactions
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00969D, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Weixiang Zhai, Yalan Feng, Huiqiang Liu, Antal Rockenbauer, Deni Mance, Shaoyong Li, Yuguang Song, Marc Baldus, Yangping Liu
The exchange (J) interaction of organic biradicals is a crucial factor controlling their physiochemical properties and potential applications, and can be modulated by changing the nature of the linker. In...
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- Acidity and basicity interplay in amides and imides self-association
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC01020J, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Wilmer Esteban Vallejo Narvaez, Eddy Ivanhoe Jimenez, Eduardo Romero-Montalvo, Arturo Sauza-de la Vega, Beatriz Quiroz-Garcia, Marcos Hernandez-Rodriguez, Tomas Rocha-Rinza
Amides dimerise more strongly than imides despite their lower acidity. Such unexpected result has been rationalised in terms of the Jorgensen Secondary Interactions Hypothesis (JSIH) that involve the spectator (C=O S )...
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- The Bethe-Salpeter Formalism with Polarisable Continuum Embedding:
Reconciling Linear-Response and State-Specific Features
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00529J, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Ivan Duchemin, Ciro Achille Achille Guido, Denis Jacquemin, Xavier Blase
The Bethe-Salpeter equation (BSE) formalism has been recently shown to be a valuable alternative to time-dependent density functional theory (TD-DFT) with the same computing time scaling with system size. In...
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- Examining the chemical and structural properties that influence the
sensitivity of energetic nitrate esters
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00903A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Virginia[space]W. Manner, Marc J. Cawkwell, Edward M. Kober, Thomas W. Myers, Geoff W. Brown, Hongzhao Tian, Christopher J. Snyder, Romain Perriot, Daniel N. Preston
The sensitivity of explosives is controlled by factors that span from intrinsic chemical reactivity to mesoscale structure, and has been a topic of extensive study for over 50 years.
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- Reversible Dispersion and Release of Carbon Nanotubes via Cooperative
Clamping Interactions with Hydrogen-bonded Nanorings
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00843D, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Raquel Chamorro, Leire de Juan-Fernandez, Belen Nieto-Ortega, Maria Jose Mayoral, Santiago Casado, Luisa Ruiz-Gonzales, Emilio M Perez, David Gonzalez Rodriguez
Due to their outstanding electronic and mechanical properties, single-walled carbon nanotubes (SWCNTs) are promising nanomaterials for the future generation of optoelectronic devices and composites. However, their scarce solubility limits their...
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- Long Distance Ion-Water Interactions in Aqueous Sulfate Nanodrops Persist
to Ambient Temperatures in the Upper Atmosphere
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00854J, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Matthew J. DiTucci, Christiane N. Stachl, Evan R Williams
The effect of temperature on the patterning of water molecules located remotely from a single SO 4 2- ion in aqueous nanodrops was investigated for nanodrops containing between 30 and 55 water...
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- Correction: Spectroscopic observation of two-center three-electron bonded
(hemi-bonded) structures of (H2S)n+ clusters in the gas phase
Abstract: Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC90072H, Correction Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Dandan Wang, Asuka Fujii
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- Construction of histidine-containing hydrocarbon stapled cell penetrating
peptides for in vitro and in vivo delivery of siRNAs
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00074C, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Soonsil Hyun, Yoonhwa Choi, Ha Neul Lee, Changki Lee, Donghoon Oh, Dong-Ki Lee, Changjin Lee, Yan Lee, Jaehoon Yu
A hydrocarbon stapled peptide, LKH-stEK, promotes delivery of nanomolar siRNAs leading to efficient gene silencing in mouse skin.
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- Iriomoteolides: novel chemical tools to study actin dynamics
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C7SC04286H, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. A. Unzue, R. Cribiu, M. M. Hoffman, T. Knehans, K. Lafleur, A. Caflisch, C. Nevado
This work broadcasts iriomoteolides as a novel and easily tunable tool for the study of actin polymerization and actin dynamics.
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- Counting Charges on Membrane-bound Peptides
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00804C, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Alicia mcGeachy, Emily Rose Caudill, Dongyue Liang, Qiang Cui, Joel A. Pedersen, Franz Geiger
Quantifying the number of charges on peptides bound to interfaces requires reliable estimates of (i) surface coverage and (ii) surface charge, both of which are notoriously difficult parameters to obtain,...
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- Competition Between Li+ and Na+ in Sodium Transporters and Receptors:
Which Na+-Binding Sites are "Therapeutic" Li+ Targets'
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05284G, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Todor Dudev, Karine Mazmanian, Carmay Lim
Sodium (Na+) acts as an indispensable allosteric regulator of the activities of biologically important neurotransmitter transporters and G-protein coupled receptors (GPCRs), which comprise well-known drug targets for psychiatric disorders and...
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- Electrochemical impedance spectroscopy of single Au nanorods
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00983J, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Tao Liu, Meng Li, Yongjie Wang, Yimin Fang, Wei Wang
We propose a monochromatic dark-field imaging microscopy (DFM) to measure the non-Faradaic electrochemical impedance spectroscopy (EIS) of single Au nanorods (AuNRs). A DFM was utilized to monitor the plasmonic scattering...
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- GO-guided direct growth of highly oriented metal-organic framework
nanosheet membranes for H2/CO2 separation
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC04815G, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yujia Li, Haiou LIU, Huanting Wang, Jieshan Qiu, Xiongfu ZHANG
Highly oriented, ultrathin metal-organic framework (MOF) membranes are attractive for practical separation applications, but the scalable preparation of such membranes especially on standard tubular supports remains a huge challenge. Here...
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- Cluster-mediated assembly enables step-growth copolymerization from binary
nanoparticle mixtures with rationally designed architectures
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00220G, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Xianfeng Zhang, Longfei Lv, Guanhong Wu, Dong Yang, Angang Dong
Directed co-assembly of binary nanoparticles (NPs) into one-dimensional copolymer-like chains is fascinating but challenging in the realm of material science. While many strategies have been developed to induce the polymerization...
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- Thermoreversible crystallization-driven aggregation of diblock copolymer
nanoparticles in mineral oil
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00762D, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Matthew J Derry, Oleksandr O Mykhaylyk, Anthony J Ryan, Steven P Armes
A poly(behenyl methacrylate)37 (PBeMA37) macromolecular chain transfer agent is utilized for the reversible addition-fragmentation chain transfer (RAFT) dispersion polymerization of benzyl methacrylate (BzMA) directly in mineral oil at 90 [degree]C....
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- Ultrathin Palladium Nanosheets with Selectively Controlled Surface Facets
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00605A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Dongdong Xu, Xiaoli Liu, Hao Lv, Ying Liu, Shulin Zhao, Min Han, Jianchun Bao, Jie He, Ben Liu
We report a facile bottom-up synthetic approach to preparing ultrathin two-dimensional (2D) palladium nanosheets (PdNSs) with selectively exposed surface facets. Our synthetic strategy is based on the utilization of the...
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- An addressable packing parameter approach for reversibly tuning the
assembly of oligo(aniline)-based supra-amphiphiles
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00068A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Wei Lyu, Maha Alotaibi, O. Alexander Bell, Kazuyoshi Watanabe, Robert Harniman, Benjamin Mark Mills, Annela Seddon, Sarah E. Rogers, Stephen M King, Wei Yan, Charl Faul
We present a newly developed approach to non-covalently address the packing parameter of an electroactive amphiphile. The pH-responsive reversible switching of a tetra(aniline)-based cationic amphiphile, TANI-pentyl trimethylammonium bromide (TANI-PTAB), between...
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- Synthesis and Applications of Nanoporous Perovskite Metal Oxides
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC03920D, Minireview Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Xiubing Huang, Guixia Zhao, Ge Wang, John Irvine
Perovskite-type metal oxides have been widely investigated and applied in various fields in the past several decades due to their extraordinary variability of compositions and structures with targeted physical and...
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- An artificial photosynthetic system for photoaccumulation of two electrons
on a fused dipyridophenazine (dppz) - pyridoquinolinone ligand
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC04348A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Jean-Francois Lefebvre, Julian Schindler, Philipp Traber, Ying Zhang, Stephan Kupfer, Stefanie Grafe, Isabelle Baussanne, Martine Demeunynck, Jean-Marie Mouesca, Serge Gambarelli, Vincent Artero, Benjamin Dietzek, Murielle Chavarot-Kerlidou
Increasing the efficiency of molecular artificial photosynthetic systems is mandatory for the construction of functional devices for solar fuels production. Decoupling the light-induced charge separation steps from the catalytic process...
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- Modified Nucleoside Triphosphates Exist in Mammals
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05472F, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Han-Peng Jiang, Jun Xiong, Fei-Long Liu, Cheng-Jie Ma, Xing-Lin Tang, Bi-Feng Yuan, Yu-Qi Feng
DNA and RNA contain diverse chemical modifications that exert important influences in a variety of cellular processes. In addition to enzyme-mediated modifications of DNA and RNA, previous in-vitro study showed...
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- Correction: Spironaphthoxazine switchable dyes for biological imaging
Abstract: Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC90071J, Correction Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yaoyao Xiong, Andreas Vargas Jentzsch, Johannes W. M. Osterrieth, Erdinc Sezgin, Igor V. Sazanovich, Katharina Reglinski, Silvia Galiani, Anthony W. Parker, Christian Eggeling, Harry L. Anderson
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- Energetic insights into two electron transfer pathways in light-driven
energy-converting enzymes
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00424B, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Keisuke Kawashima, Hiroshi Ishikita
We report redox potentials ( E m ) for one-electron reduction for all chlorophylls in the two electron-transfer branches of, water-oxidizing enzyme photosystem II (PSII), photosystem I (PSI), and purple bacterial photosynthetic reaction...
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- Elements of fractal geometry in the 1H NMR spectrum of a copolymer
intercalation-complex: identification of the underlying Cantor set
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00830B, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. John S. Shaw, Rajendran Vaiyapuri, Matthew P. Parker, Claire A. Murray, Kate J. C. Lim, Cong Pan, Marcus Knappert, Christine J. Cardin, Barnaby W. Greenland, Ricardo Grau-Crespo, Howard M. Colquhoun
Intercalation of pyrene into the chain-folds of a binary copolyimide results in a self-similar 1 H NMR spectrum.
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- Protein surface functionalisation as a general strategy for facilitating
biomimetic mineralisation of ZIF-8
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00825F, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Natasha K. Maddigan, Andrew Tarzia, David M. Huang, Christopher J. Sumby, Stephen G. Bell, Paolo Falcaro, Christian. J. Doonan
The surface charge and chemistry of a protein determines its ability to facilitate biomimetic mineralisation.
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- The enhancement and suppression of immersion mode heterogeneous
ice-nucleation by solutes
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05421A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Thomas Francis Whale, Mark Andrew Holden, Theodore William Wilson, Daniel O'Sullivan, Benjamin John Murray
Heterogeneous nucleation of ice from aqueous solutions is an important yet poorly understood process in multiple fields, not least the atmospheric sciences where it impacts the formation and properties of...
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- Stabilizing Fleeting Intermediates of Stilbene Photocyclization with
Amino-Borane Functionalization: The Rare Isolation of Persistent
Dihydrophenanthrenes and Their [1,5] H-Shift Isomers
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00560E, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Yong-gang Shi, Soren K Mellerup, Kang Yuan, Guofei Hu, Francoise sauriol, Tai Peng, Nan Wang, Pangkuan Chen, Suning Wang
The key intermediate, 4a,4b-dihydrophenanthrene (DPH), involved in the photocyclization of stilbene and derivatives is known to be unstable, and is therefore pooly characterized/understood. We have found that functionalizing stilbenes with...
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- Pd(II)-Catalyzed Synthesis of Bifunctionalized Carboranes via Cage B-H
Activation of 1-CH2NH2-o-carboranes
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC01154K, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Xiaolei Zhang, Hong Yan
Aminoalkyl carboranes are anticipated to be valuable synthons toward the synthesis of bifunctnioalized carboranes. However, direct cage boron derivation of these carborane derivatives has not been solved. Herein, the reversible...
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- Reactivity Enhancement of a Diphosphene by Reversible N-Heterocyclic
Carbene Coordination
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00348C, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Debabrata Dhara, Pankaj Kalita, Subhadip Mondal, Suriya Narayanan, Kaustubh Mote, Volker Huch, Michael Zimmer, Cem Burak Burak Yildiz, David Scheschkewitz, Vadapalli Chandrasekhar, Anukul Jana
Diphosphene Ter Mes P=PTer Mes ( 1 ; Ter Mes = 2,6-Mes 2 C 6 H 3 ; Mes = 2,4,6-Me 3 C 6 H 2 ) and NHC Me4 2 (NHC Me4 = 1,3,4,5-tetramethylimidazol-2-ylidene) exist in an equilibrium mixture with the NHC Me4 -coordinated diphosphene 3 . While uncoordinated 1 is inert...
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- Cyclometalated Gold(III) Complexes: Noticeable Differences between (N,C)
and (P,C) Ligands in Migratory Insertions
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC04899H, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Jordi Serra, Pau Font, E. Daiann Sosa Carrizo, Sonia Ladeira, Stephane Massou, Teodor Parella, Karinne Miqueu, Abderrahmane Amgoune, Xavi Ribas, Didier Bourissou
Gold(III) complexes are garnering increasing interest for opto-electronic, therapeutic and catalytic applications. But so far, very little is known about the factors controlling their reactivity and the very influence of...
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- How does chiral self-sorting take place in the formation ofhomochiral
Pd6L8 capsules consisting of cyclotriveratrylene-basedchiral tritopic
ligands'
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC01062E, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Shumpei Kai, Tatsuo Kojima, Flora Thorp-Greenwood, Michaele Hardie, Shuichi Hiraoka
The chiral self-sorting process during the self-assembly of homochiral Pd6L8 capsules from cyclotriveratrylene (CTV)-based chiral tritopic ligands (L) and PdPy*4(OTf)2 (Py*: 3- chloropyridine) was investigated by NMR-based approach (QASAP: quantitative...
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- Through Tissue Imaging of a Live Breast Cancer Tumour Model Using Handheld
Surface Enhanced Spatially Offset Resonance Raman Spectroscopy
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00994E, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Fay Nicolson, Lauren E Jamieson, Samuel Mabbott, Konstantinos Plakas, Neil Shand, Michael Detty, Duncan Graham, Karen Faulds
In order to improve patient survival and reduce the amount of unnecessary and traumatic biopsies, non-invasive detection of cancerous tumours is of imperative and urgent need. Multicellular tumour spheroids (MTS)...
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- Transition-Metal-Free Decarboxylative Bromination of Aromatic Carboxylic
Acids
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC01016A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Jacob Quibell, Gregory Perry, Diego Cannas, Igor Larrosa
Methods for the conversion of aliphatic acids to alkyl halides have progressed significantly over the past century, however, the analogous decarboxylative bromination of aromatic acids has remained a longstanding challenge....
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- Experiments indicating a second hydrogen ordered phase of ice VI
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00135A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Tobias M. Gasser, Alexander Valentin Thoeny, Lucie J Plaga, Karsten W Koster, Martin Etter, Roland Bohmer, Thomas Loerting
In the last twelve years five new ice phases were experimentally prepared. Two of them are empty clathrate hydrates and three of them represent hydrogen ordered counterparts of previously known...
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- Molecular mechanism of lytic polysaccharide monooxygenases
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00426A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Erik Donovan Hedegard, Ulf Ryde
The lytic polysaccharide monooxygenases (LPMOs) are copper metalloenzymes that can enhance polysaccharide depolymerization through an oxidative mechanism and hence boost generation of biofuel from e.g. cellulose. By employing density functional...
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- Self-complementary nickel halides enable multifaceted comparisons of
intermolecular halogen bonds: fluoride ligands vs other halides
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00890F, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Vargini Thangavadivale, Pedro Aguiar, Naseralla A Jasim, Sarah Pike, Dan Smith, Adrian C. Whitwood, Lee Brammer, Robin Perutz
The syntheses of three series of complexes designed with self-complementary motifs for formation of halogen bonds between an iodotetrafluorophenyl ligand and a halide ligand at square-planar nickel are reported, allowing...
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- Correction: Anisotropy of CoII transferred to the Cr7Co polymetallic
cluster via strong exchange interactions
Abstract: Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC90065E, Correction Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Elena Garlatti, Tatiana Guidi, Alessandro Chiesa, Simon Ansbro, Michael L. Baker, Jacques Ollivier, Hannu Mutka, Grigore A. Timco, Inigo Vitorica-Yrezabal, Eva Pavarini, Paolo Santini, Giuseppe Amoretti, Richard E. P. Winpenny, Stefano Carretta
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- Topotactic Anion-exchange in Thermoelectric Nanostructured Layered Tin
Chalcogenides with Reduced Selenium Content
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05190E, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Guang Han, Srinivas Popuri, Heather Greer, Ruizhi Zhang, Lourdes Ferre Llin, Jan-Willem Bos, Wuzong Zhou, Mike Reece, Douglas Paul, Andrew Knox, Duncan Gregory
Anion exchange has been performed with nanoplates of tin sulfide (SnS) via "soft chemical" organic-free solution syntheses to yield layered pseudo-ternary tin chalcogenides on a 10 g-scale. SnS undergoes a...
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- Chiral Macrocyclic Terpyridine Complexes
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05285E, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Thomas Brandl, Viktor Hoffmann, Andrea Pannwitz, Daniel Haussinger, Markus Neuburger, olaf fuhr, Stefan Bernhard, Oliver S. Wenger, Marcel Mayor
A new family of compact and chiral M(II) bis(terpyridine) complexes is presented. The peripheral decoration of the terpyridine ligand system with ortho-ethynylphenyl substituents in 4 and 4'' positions enables the...
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- C-H activation and nucleophilic substitution in a photochemically
generated high valent iron complex
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05378A, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Jia Hui Lim, Xenia Engelmann, Sacha Corby, Rakesh Ganguly, Kallol Ray, Han Sen Soo
The photochemical oxidation of a (TAML)Fe III complex 1 using visible light generated Ru(bpy) 3 3+ produces valence tautomers (TAML)Fe IV ( 1 + ) and (TAML[round bullet, filled] + )Fe III ( 1-TAML[round bullet, filled] + ), depending on the exogenous anions. The presence of labile...
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- Experimental and theoretical evidence of a supercritical-like transition
in an organic semiconductor presenting colossal uniaxial negative thermal
expansion
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00159F, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Arie van der Lee, Gille H. Roche, Guillaume Wantz, Joel J.E. Moreau, olivier joseph DAUTEL, Jean-Sebastien Filhol
Thermal expansion coefficients of most materials are usually small, typically up to 50 parts per million per Kelvin, and positive, i.e. materials expand when heated. Some materials show atypical behavior...
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- Precise control of pore hydrophilicity enabled by post-synthetic cation
exchange in metal-organic frameworks
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00112J, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Ashley M Wright, Adam J Rieth, Sungwoo Yang, Evelyn Wang, Mircea Dinca
The ability to control the relative humidity at which water uptake occurs in a given adsorbent is advantageous, making that material applicable to a variety of different applications. Here, we...
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- Highly Luminescent, Biocompatible Ytterbium(III) Complexes as
Near-Infrared Fluorophores for Living Cell Imaging
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00259B, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yingying Ning, Juan Tang, Yi-Wei Liu, Jing Jing, Yuansheng Sun, Jun-Long Zhang
Herein, we report the design and synthesis of biocompatible Yb 3+ complexes for near-infrared (NIR) living cell imaging. In addition to high NIR luminescence (quantum yields up to 23% and 13%...
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- Gene specific-loci quantitative and single-base resolution analysis of
5-formylcytosine by compound-mediated polymerase chain reaction
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00493E, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Xiang Zhou, Yafen Wang, Chaoxing Liu, Xiong Zhang, Wei Yang, Fan Wu, Guangrong Zhou, Xiaocheng Weng
5-formylcytosine (5fC) is known as one of the key players in the process of active DNA demethylation and displays essential epigenetic functions in mammals. In spite of the blooming development...
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- A Redox-Active Diborane Platform Performs C(sp3)‒H Activation and
Nucleophilic Substitution Reactions
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00743H, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Thomas Kaese, Timo Trageser, Hendrik Budy, Michael Bolte, Hans-Wolfram Lerner, Matthias Wagner
Organoboranes are among the most versatile and widely used reagents in synthetic chemistry. A significant further expansion of their application spectrum would be achievable if boron-containing reactive intermediates capable of...
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- Mechano-induced persistent room-temperature phosphorescence from purely
organic molecule
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00429C, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Yingxiao Mu, Zhiyong Yang, Junru Chen, Zhan Yang, Wenlang Li, Xianbao Tan, Zhu Mao, Tao Yu, Juan Zhao, Shizhao Zheng, Siwei Liu, Yi Zhang, Zhenguo Chi, Jiarui Xu, Matthew Phillip Aldred
Persistent room-temperature phosphorescence (RTP) of purely organic materials in the solid-state has recently attracted much research interest and found promising rapid and visual applications by naked eyes, after the removal...
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- Simulations of synthesis of the boron-nitride nanostructures in a hot,
high pressure gas volume
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00667A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Predrag Krstic, Longtao Han, Stephan Irle, Hiromi Nakai
We performed nanosecond timescale computer simulations of clusterization and agglomeration processes of boron nitride (BN) nanostructures in hot, high pressure gas, starting from eleven different atomic and molecular precursor systems...
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- Covalent triazine framework modified with coordinatively-unsaturated Co or
Ni atoms for CO2 electrochemical reduction
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00604K, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Panan Su, Kazuyuki Iwase, Takashi Harada, Kazuhide Kamiya, Shuji Nakanishi
The electrochemical reduction of carbon dioxide (CO 2 ) has attracted considerable attention as a means of maintaining the carbon cycle. This process still suffers from poor performance,including low faradaic efficiencies and...
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- Macrophage-Mediated Delivery of Light Activated Nitric Oxide Prodrugs with
Spatial, Temporal and Concentration Control
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00015H, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Michael Evans, Po-Ju Huang, Yuji Iwamoto, Kelly Ibsen, Emory Ming-Yue Chan, Yutaka Hitomi, Peter C Ford, Samir Mitragotri
Nitric oxide (NO) holds great promise as a treatment for cancer hypoxia, if its concentration and localization can be precisely controlled. Here, we report a "Trojan Horse" strategy to provide...
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- Crystal structure and functional analysis of large-terpene synthase
belonging to a newly found subclass
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00289D, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Masahiro Fujihashi, Tsutomu Sato, Yuma Tanaka, Daisuke Yamamoto, Tomoyuki Nishi, Daijiro Ueda, Mizuki Murakami, Yoko Yasuno, Ai Sekihara, Kazuma Fuku, Tetsuro Shinada, Kunio Miki
Thousands of terpenes have been identified to date. However, only two classes of enzymes are known to be involved in their biosynthesis, and each class has characteristic amino-acid motifs. We...
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- Synthetic glycan-based TLR4 agonists targeting Caspase-4/11 for the
development of adjuvants and immunotherapeutics
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05323A, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Florian Adanitsch, Jianjin Shi, Feng Shao, Rudi Beyaert, Holger Heine, Alla Zamyatina
Gram-negative bacterial lipopolysacchartide (LPS)-induced Toll-like receptor 4 (TLR4) mediated pro-inflammatory signaling plays a key role in immunoprotection against infectious challenge and boosts the adaptive immunity, whereas the activation of cytosolic...
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- Using stereoretention for the synthesis of E-macrocycles with
ruthenium-based olefin metathesis catalysts
Abstract:Chem. Sci. , 2018, Advance Article
DOI : 10.1039/C8SC00435H, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Tonia S. Ahmed, T. Patrick Montgomery, Robert H. Grubbs
The synthesis of E -macrocycles is achieved using stereoretentive, Ru-based olefin metathesis catalysts supported by dithiolate ligands.
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- "Waiting" Carbon Nitride Radical Anion: Charge Storage Material and Key
Intermediate in Direct C-H Thiolation of Methylarenes Using Elemental
Sulfur as "S"-source
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00745D, Edge Article Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence. Aleksandr Savateev, Bogdan Kurpil, Artem Mishchenko, Guigang Zhang, Markus Antonietti
Potassium poly(heptazine imide), a carbon nitride based semiconductor with high structural order and valence band potential of +2.2 V vs. NHE, in the presence of hole scavengers and under visible...
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- Identifying key descriptors in surface binding: Interplay of surface
anchoring and intermolecular interactions for carboxylates on Au(110)
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05313D, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Christopher R. O'Connor, Fanny Hiebel, Wei Chen, Efthimios Kaxiras, Robert James Madix, Cynthia Friend
The relative stability of carboxylates on Au(110) was investigated as part of a comprehensive study of adsorbate binding on Group IB metals that can be used to predict and understand...
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- Anisotropy of CoII transferred to the Cr7Co polymetallic cluster via
strong exchange interactions
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00163D, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Elena Garlatti, Tatiana Guidi, Alessandro Chiesa, Simon Ansbro, Michael Baker, Jacques Ollivier, Hannu Mutka, Grigore A. Timco, Inigo Vitorica-Yrzebal, Eva Pavarini, Paolo Santini, Giuseppe Amoretti, Richard E. P. Winpenny, Stefano Carretta
The Cr7Co ring represents a model system to understand how the anisotropy of a CoII ion is transferred to the effective anisotropy of a polymetallic cluster by strong exchange interactions....
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- Spin states, vibrations and spin relaxation in molecular nanomagnets and
spin qubits: a critical perspective
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C7SC05464E, Perspective Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Luis Escalera-Moreno, Jose J. Baldovi, Alejandro Gaita-Arino, Eugenio Coronado
Very recently the closely related fields of molecular spin qubits, single ion magnets and single atom magnets have suffered a convulsion. We have witnessed a jump in the phase memory...
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- A pre-protective strategy for precise tumor targeting and efficient
photodynamic therapy with a switchable DNA/upconversion nanocomposite
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00098K, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Zhengze Yu, Yegang Ge, Qiaoqiao Sun, Wei Pan, Xiuyan Wan, Na Li, Bo Tang
Tumor-specific targeting based on folic acid (FA) is one of the most common and significant approaches in cancer therapy. However, the expression of folate receptors (FRs) in normal tissues will...
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- Developing Structure-Property Relationship to Design Solid State
Multi-stimuli Responsive Materials and Their Potential Applications in
Different Fields
Abstract: Chem. Sci. , 2018, Accepted Manuscript
DOI : 10.1039/C8SC00143J, Edge Article Open Access This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. Partha Hazra, Bibhisan Roy, Mallu Chenna Reddy
Prediction of multi-stimuli responsive behavior in newly developed luminogen is an appealing yet challenging puzzle, since no concrete design strategy has been developed so far. In this article, we demonstrate...
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